反应条件
1: borane-THF; boric acid trimethyl ester; (S)-(-)-α,α-diphenyl-2-pyrrolidinemethanol / tetrahydrofuran / 3 h / 0 - 25 °C 2: methanesulfonyl chloride / dichloromethane / 2 h / -10 °C 3: Wilkinson's catalyst / water; acetonitrile / 5 h / Inert atmosphere; Reflux View Scheme
参考文献
Periasamy, Mariappan; Sanjeevakumar, Nalluri; Dalai, Manasi; Gurubrahamam, Ramani; Reddy, Polimera Obula
Organic Letters, 2012 , vol. 14, # 12 p. 2932 - 2935