反应条件
1: 2-ethynyl-2-phenyl-[1,3]dithiolane With methyl-magnesium iodide in diethyl ether
T=20°C; 0.5 h;
2: 1-(iodo)-4-methylbenzene With triphenylphosphine; tris(dibenzylideneacetone)dipalladium (0) in tetrahydrofuran; diethyl ether
Kumada-Corriu cross-coupling; Heating; Further stages.;
参考文献
Huang, Li-Fu; Lee, Chin-Fa; Tseng, Jui-Chang; Luh, Tien-Yau
Synlett, 2006 , # 18 p. 3173 - 3175