1: 1H-imidazole With potassium tert-butylate in dimethyl sulfoxide 0.0833333 h; 2: 1-fluoro-2-nitro-4-trifluoromethylbenzene in dimethyl sulfoxide T=20°C; 0.341667 h;
参考文献
CANCER RESEARCH TECHNOLOGY LIMITED; INSTITUTE OF CANCER RESEARCH: ROYAL CANCER HOSPITAL (THE)
Patent: WO2009/77766 A1, 2009 ;
Location in patent: Page/Page column 196 ;
WO 2009/077766 A1
1: 63 percent / Fe powder; HOAc / propan-2-ol / 1.5 h / Heating
2: pyridine / 3.5 h / -5 - 20 °C
View Scheme
参考文献
Ivanov, Vladimir V.; Yurchenko, Alexandr A.; Chernega, Alexander N.; Pinchuk, Alexandr M.; Tolmachev, Andrej A.
Heteroatom Chemistry, 2002 , vol. 13, # 1 p. 84 - 92
