3,4-二羟基苯乙酸甲酯合成路线 (共 17 条)
反应条件
hydrogenchloride; hydrogen; 5 ruthenium on carbon in water T=55°C; P=18751.9 Torr; 26 h; Product distribution / selectivity;
参考文献
DSM IP ASSETS B.V.
Patent: WO2007/9590 A1, 2007 ;
Location in patent: Page/Page column 3 ;
反应条件
Agaricus bisporus; oxygen in aq. phosphate buffer; dichloromethane T=25°C; pH=7; 24 h;
参考文献
Bozzini, Tiziana; Botta, Giorgia; Delfino, Michela; Onofri, Silvano; Saladino, Raffaele; Amatore, Donatella; Sgarbanti, Rossella; Nencioni, Lucia; Palamara, Anna Teresa
Bioorganic and Medicinal Chemistry, 2013 , vol. 21, # 24 p. 7699 - 7708
反应条件
hydrogenchloride; hydrogen; palladium over charcoal in methanol T=40°C; P=7500.75 Torr; 20 h; Product distribution / selectivity;
参考文献
DSM IP ASSETS B.V.
Patent: WO2007/9590 A1, 2007 ;
Location in patent: Page/Page column 9 ;
反应条件
sodium carbonate in methanol; water
反应条件
sulfuric acid 2 h; RefluxDarknessInert atmosphere;
参考文献
Geiseler, Bianca; Fruk, Ljiljana
Journal of Materials Chemistry, 2012 , vol. 22, # 2 p. 735 - 741
反应条件
1: chloro-trimethyl-silane / 24 h / 25 °C 2: Agaricus bisporus; oxygen / aq. phosphate buffer; dichloromethane / 24 h / 25 °C / pH 7 View Scheme
参考文献
Bioorganic and Medicinal Chemistry, , vol. 21, # 24 p. 7699 - 7708
反应条件
cesium fluoride in N,N-dimethyl-formamide 3 h; Heating;
参考文献
Journal of Medicinal Chemistry, , vol. 44, # 11 p. 1794 - 1801
参考文献
Kindler
Chemische Berichte, 1941 , vol. 74, p. 315,316
反应条件
1: 55 percent / CsF / dimethylformamide / 3 h / Heating 2: 97 percent / 20percent aq. KOH / methanol / 3 h / Heating View Scheme
参考文献
Cabedo; Andreu; Ramirez de Arellano; Chagraoui; Serrano; Bermejo; Protais; Cortes
Journal of Medicinal Chemistry, 2001 , vol. 44, # 11 p. 1794 - 1801
反应条件
1: K2CO3 / acetone 2: LiAlH4 View Scheme
参考文献
Burger, Johann F. W.; Brandt, E. Vincent; Ferreira, Daneel
Phytochemistry (Elsevier), 1987 , vol. 26, # 5 p. 1453 - 1458