in neat (no solvent) absence of air and moisture; distn. of excess of BrF5 on IO2F3, warming to -18°C then to room temp. (40 min); product mixt. not sepd., detd. by (19)F NMR and Raman spectroscopy;

in neat (no solvent) absence of air and moisture; distn. of excess of BrF5 on IO2F3, warming to -18°C then to room temp. (40 min); product mixt. not sepd., detd. by (19)F NMR and Raman spectroscopy;

in neat (no solvent) absence of air and moisture; distn. of excess of BrF5 on IO2F3, warming to -18°C then to room temp. (40 min); product mixt. not sepd., detd. by (19)F NMR and Raman spectroscopy;