反应条件
1.1: palladium diacetate; silver(l) oxide; potassium acetate / N,N-dimethyl-formamide / 110 °C
2.1: lithium aluminium tetrahydride / diethyl ether / 3 h / 20 °C / |Cooling with ice
2.2: 0.5 h / |Cooling with ice
3.1: pyridine; trimethylsilyl iodide / sulfolane / 20 h / 70 °C / |Inert atmosphere
4.1: sodium hydroxide; oxygen / water; acetone / 18 h / 20 °C
5.1: hydrogenchloride / tetrahydrofuran / 20 h / 60 °C
View Scheme
参考文献
Ramkumar, Nagarajan; Nagarajan, Rajagopal
Journal of Organic Chemistry, 2013 , vol. 78, # 6 p. 2802 - 2807
