3-(4-甲氧基苯基)-丙酰胺合成路线 (共 30 条)
反应条件
1: sulfur; benzene / 135 °C 2: aq.-ethanolic KOH-solution 3: 210 °C / Erhitzen im Ammoniak-Strom View Scheme
参考文献
Kindler; Peschke
Archiv der Pharmazie (Weinheim, Germany), 1932 , vol. 270, p. 353,359
参考文献
Behringer et al.
Chemische Berichte, 1958 , vol. 91, p. 2773,2783
反应条件
1: sodium amalgam 2: thionyl chloride; chloroform / nachfolgend Behandlung mit Natriumhydroxyd in Ammoniak View Scheme
参考文献
Callow; Gulland; Haworth
Journal of the Chemical Society, 1929 , p. 1448
反应条件
1: potassium hypobromite / 55 °C 2: sodium acetate 3: sodium; xylene / Behandeln der Reaktionsloesung mit Methyljodid 4: hydriodic acid 5: concentrated hydrochloric acid / 170 °C View Scheme
参考文献
Walpole
Journal of the Chemical Society, 1910 , vol. 97, p. 946
反应条件
1: bromine; NaOH-solution / 55 °C 2: hydrobromic acid / 160 °C View Scheme
参考文献
Barger; Walpole
Journal of the Chemical Society, 1909 , vol. 95, p. 1722
反应条件
1: potassium hypobromite / 55 °C 2: sodium acetate 3: sodium; xylene / Behandeln der Reaktionsloesung mit Methyljodid 4: hydriodic acid 5: concentrated hydrochloric acid / 170 °C 6: methanol View Scheme
参考文献
Walpole
Journal of the Chemical Society, 1910 , vol. 97, p. 946
反应条件
1: phosphorus (V)-oxide; xylene 2: HCl; SnCl2; diethyl ether / und Erwaermen des Reaktionsprodukts mit wss.Na2CO3-Loesung View Scheme
参考文献
Evans; Walker
Journal of the Chemical Society, 1947 , p. 1571
反应条件
sodium hydroxide; bromine in water T=70 - 80°C; 0.25 h;
参考文献
Zhuangyu, Zhang; Yi, Pan; Hongwen, Hu; Tsi-yu, Kao
Synthetic Communications, 1990 , vol. 20, # 22 p. 3563 - 3574
参考文献
Barger; Walpole
Journal of the Chemical Society, 1909 , vol. 95, p. 1722
参考文献
Ramart-Lucas; Amagat
Bulletin de la Societe Chimique de France, 1932 , vol. <4> 51, p. 108,117