1-(2-氨基-5-甲基苯基)乙酮合成路线 （共 15 条）
反应条件
T=18 - 20°C; 24 h; Irradiationon silica gel, competing reaction; Product distribution;
参考文献
Magdy, M.; Malik, Abdel-; Mayo, Paul de
Canadian Journal of Chemistry, 1984 , vol. 62, p. 1275 - 1278
反应条件
hydrogenchloride in water; toluene
参考文献
Kirin Beer Kabushiki Kaisha
Patent: US6187926 B1, 2001 ;
反应条件
iron sulphate heptahydrate; sodium meta-nitrobenzenesulfonic acid in methanesulfonic acid T=120°C; Inert atmosphere;
参考文献
Wang, Jingjing; Chen, Weiqiang; Zuo, Sujing; Liu, Lu; Zhang, Xinrui; Wang, Jianhui
Angewandte Chemie - International Edition, 2012 , vol. 51, # 49 p. 12334 - 12338
Angew. Chem., 2012 , vol. 124, # 49 p. 12500 - 12504,5
反应条件
hydrogenchloride in water; toluene
参考文献
Kirin Beer Kabushiki Kaisha
Patent: US6187926 B1, 2001 ;
反应条件
1: AcOH / ethanol / 6 h / Heating
2: methanesulfonic acid; P2O5 / 0.5 h / 80 °C
3: 72 percent / AcOH / 2 h / Heating
View Scheme
参考文献
Bergman, Jan; Engqvist, Robert; Stalhandske, Claes; Wallberg, Hans
Tetrahedron, 2003 , vol. 59, # 7 p. 1033 - 1048
