2,6-二甲基-4-羟基喹啉合成路线 (共 5 条)
反应条件
toluene-4-sulfonic acid in hexane; ethyl acetate; benzene
参考文献
Lin, Chu-Chung; Liu, Jen-Fuh; Chang, Chih-Wei; Chen, Shu-Jen; Xiang, Yibin; Cheng, Pei-Chin; Jan, Jiing-Jyh
Patent: US2004/209902 A1, 2004 ;
US 20040209902 A1
反应条件
NaHSO4 on SiO2 solid support 0.0833333 h; Microwave irradiationNeat (no solvent);
参考文献
Sapkal, Suryakant B.; Shelke, Kiran F.; Shingate, Bapurao B.; Shingare, Murlidhar S.
Journal of the Korean Chemical Society, 2010 , vol. 54, # 6 p. 723 - 726
反应条件
0.0383333 h; microwave irradiation;
参考文献
Nadaraj; Selvi, S. Thamarai
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 2007 , vol. 46, # 7 p. 1203 - 1207
反应条件
N,N-dimethyl-aniline; phosphorus oxytribromide in toluene T=90°C; 3.5 h;
参考文献
Warner; Barker; Jackman; Burrows; Roberts; Bishop; O'Connor; Hughes
Journal of Medicinal Chemistry, 1992 , vol. 35, # 15 p. 2761 - 2768
反应条件
N,N-dimethyl-aniline; trichlorophosphate in toluene
T=90°C; 3.5 h;
参考文献
Warner; Barker; Jackman; Burrows; Roberts; Bishop; O'Connor; Hughes
Journal of Medicinal Chemistry, 1992 , vol. 35, # 15 p. 2761 - 2768