α-(三甲基硅氧基)苯乙腈合成路线 (共 67 条)
反应条件
Sm{N(SiMe3)2}3 in tetrahydrofuran T=0°C; 4 h;
参考文献
Iwanami, Katsuyuki; Aoyagi, Masaru; Oriyama, Takeshi
Tetrahedron Letters, 2005 , vol. 46, # 44 p. 7487 - 7490
反应条件
Amberlite XAD-2 resin in acetonitrile T=60°C; 8 h;
参考文献
Sukata, Kazuaki
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 10 p. 3820 - 3822
反应条件
(CF3SO2)2NSiMe3 in dichloromethane T=-78°C; 0.25 h;
参考文献
Kaur, Harpinder; Kaur, Gurmeet; Trehan, Sanjay
Synthetic Communications, 1996 , vol. 26, # 10 p. 1925 - 1929
反应条件
1H-imidazole; 4-(N,N-dimethlyamino)pyridine in diethyl ether
参考文献
Jackson, W. Roy; Jacobs, Howard A.; Jayatilake, Gamini S.; Matthews, Barry R.; Watson, Keith G.
Australian Journal of Chemistry, 1990 , vol. 43, # 12 p. 2045 - 2062
反应条件
lithium diisopropyl amide in tetrahydrofuran T=-78 - 20°C;
参考文献
Angewandte Chemie - International Edition, , vol. 42, # 45 p. 5613 - 5615
反应条件
1: N-methylmorpholine N-oxide / polyaniline-supported Os complex / acetone; acetonitrile; H2O / 3 h / 20 °C 2: 99 percent / polyaniline-supported Sc complex / CH2Cl2 / 1 h / 20 °C View Scheme
参考文献
Advanced Synthesis and Catalysis, , vol. 348, # 12-13 p. 1734 - 1742
反应条件
in acetonitrile T=30°C; Strecker reaction; P=6000480 Torr; 24 h;
参考文献
Heterocycles, , vol. 66, # 1 p. 675 - 681
反应条件
1-methyl-3-(4-nitrobenzyl)imidazolium hexafluorophosphate T=20°C; 1 h; Ionic liquid;
参考文献
Ren, Yajun; Li, Minghao; Yang, Jie; Peng, Jiajian; Gu, Yanlong
Advanced Synthesis and Catalysis, 2011 , vol. 353, # 18 p. 3473 - 3484
反应条件
trimethylsilyl trifluoromethanesulfonate; triethylamine in dichloromethane T=20°C; 15 h; Yield given. Yields of byproduct given;
参考文献
Tetrahedron Letters, , vol. 36, # 10 p. 1653 - 1656
反应条件
in tetrahydrofuran 1 h; Ambient temperature;
参考文献
Yoneda, Ryuji; Santo, Kazunori; Harusawa, Shinya; Kurihara, Takushi
Synthesis, 1986 , # 12 p. 1054 - 1055