5,10,15,20-四(五氟苯基)卟啉合成路线 （共 31 条）
反应条件
1: With methanesulfonic acid in dichloromethane 0.5 h; 2: With 2,3-dicyano-5,6-dichloro-p-benzoquinone in dichloromethane 0.5 h;
参考文献
Angewandte Chemie - International Edition, , vol. 45, # 19 p. 3150 - 3154
反应条件
1: With scandium tris(trifluoromethanesulfonate) in dichloromethane T=20°C; 2: With 2,3-dicyano-5,6-dichloro-p-benzoquinone in dichloromethane T=20°C; 3: With triethylamine in dichloromethane T=20°C;
参考文献
Journal of Organic Chemistry, , vol. 75, # 3 p. 553 - 563
反应条件
1: With H(COOEt)3; boron trifluoride diethyl etherate in chloroform T=20°C; Condensation; 1.25 h; 2: With 2,3-dicyano-5,6-dichloro-p-benzoquinone in chloroform Oxidation;
参考文献
Journal of the Chemical Society. Perkin Transactions 2, , # 10 p. 2221 - 2226
反应条件
1: With boron trifluoride diethyl etherate in chloroform T=20°C; 3.5 h; 2: With triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone in chloroform T=20°C; 3 h;
参考文献
Collman, James P.; Zeng, Li; Wang, Hong J. H.; Lei, Aiwen; Brauman, John I.
European Journal of Organic Chemistry, 2006 , # 12 p. 2707 - 2714
反应条件
1: With methanesulfonic acid in dichloromethane 2 h; 2: With 2,3-dicyano-5,6-dichloro-p-benzoquinone in dichloromethane T=20°C; Further stages. Further byproducts.;
参考文献
Chemistry - A European Journal, , vol. 13, # 5 p. 1620 - 1628
反应条件
1: With boron trifluoride diethyl etherate in dichloromethane T=20°C; Cyclization; 1.33333 h; 2: With 2,3-dicyano-5,6-dichloro-p-benzoquinone in dichloromethane T=20°C; Oxidation; 1 h;
参考文献
Tetrahedron, , vol. 55, # 22 p. 6771 - 6784
反应条件
propionic acid 13 h;
参考文献
Hosseini, Ali; Taylor, Steven; Accorsi, Gianluca; Armaroli, Nicola; Reed, Christopher A.; Boyd, Peter D. W.
Journal of the American Chemical Society, 2006 , vol. 128, # 49 p. 15903 - 15913
反应条件
1: With acetic acid 2 h; Heating / reflux; 2: With ammonia; water
参考文献
US6730666 B1, ;
Page/Page column 15; 16 ;
US 6730666 B1
反应条件
1: With boron trifluoride diethyl etherate in dichloromethane T=20°C; Cyclization; 1.33333 h; 2: With 2,3-dicyano-5,6-dichloro-p-benzoquinone in dichloromethane T=20°C; Oxidation; 1 h;
参考文献
Tetrahedron, , vol. 55, # 22 p. 6771 - 6784
反应条件
1: With methanesulfonic acid in dichloromethane T=0°C; 2 h; Inert atmosphere; 2: With 2,3-dicyano-5,6-dichloro-p-benzoquinone in dichloromethane 10 h; Inert atmosphere;
参考文献
European Journal of Organic Chemistry, , # 8 p. 1341 - 1349
