5,10,15,20-四(五氟苯基)卟啉合成路线 （共 31 条）
反应条件
1: With boron trifluoride diethyl etherate; 2,2-dimethoxy-propane in dichloromethane Condensation; 1.5 h; 2: With 2,3-dicyano-5,6-dichloro-p-benzoquinone in dichloromethane; toluene Oxidation; 5 h;
参考文献
Journal of Physical Chemistry A, , vol. 103, # 49 p. 10540 - 10552
反应条件
boron trifluoride diethyl etherate in ethanol; dichloromethane Ambient temperature;
参考文献
Journal of Organic Chemistry, , vol. 60, # 6 p. 1554 - 1564
反应条件
1: With boron trifluoride diethyl etherate in dichloromethane T=2°C; 20 h; Inert atmosphere; 2: With 2,3-dicyano-5,6-dichloro-p-benzoquinone in dichloromethane 0.25 h; Inert atmosphere;
参考文献
Chemistry - A European Journal, , vol. 19, # 1 p. 338 - 349
反应条件
pyrrole; acetic acid in nitrobenzene Reflux;
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 24, # 3 p. 808 - 812
反应条件
1: With boron trifluoride diethyl etherate in chloroform 2: With 2,3-dicyano-5,6-dichloro-p-benzoquinone in chloroform Further byproducts given;
参考文献
Lash, Timothy D.; Colby, Denise A.; Ferrence, Gregory M.
European Journal of Organic Chemistry, 2003 , # 23 p. 4533 - 4548
反应条件
propionic acid T=150°C; 1.5 h;
参考文献
Journal of Porphyrins and Phthalocyanines, , vol. 14, # 11 p. 975 - 984
反应条件
boron trifluoride diethyl etherate; chloranil 1.) CH2Cl2, r.t., 1 h, 2.) reflux, 1 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Journal of Organic Chemistry, , vol. 59, # 26 p. 8312 - 8315
反应条件
methanesulfonic acid; 2,3-dicyano-5,6-dichloro-p-benzoquinone in dichloromethane T=0°C; 2 h; Product distribution; Further Variations:ReagentsTemperatures;
参考文献
Tetrahedron Letters, , vol. 44, # 12 p. 2505 - 2507
反应条件
boron trifluoride diethyl etherate; chloranil; 4-formylbenzoic acid methyl ester 1.) 37 deg C, 40 h, 2.) 37 deg C, 3 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 68, # 7 p. 1959 - 1968
反应条件
boron trifluoride diethyl etherate; chloranil 1.) 37 deg C, 40 h, 2.) 37 deg C, 3 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 68, # 7 p. 1959 - 1968
