1: 2-[(11-bromoundecyl)oxy]tetrahydro-2H-pyran With magnesium in tetrahydrofuran
2: (S)-4-methyltetradecyl tosylate With dilithium tetrachlorocuprate in tetrahydrofuran
T=-78 - 20°C;
3: With ammonium chloride in tetrahydrofuran; water
cooling; Title compound not separated from byproducts;
参考文献
Mori, Kenji
Bioscience, Biotechnology and Biochemistry, 2003 , vol. 67, # 10 p. 2224 - 2231