1-溴-4-(甲氧基甲氧基)苯合成路线 （共 19 条）
反应条件
potassium carbonate in acetone 2 h; Heating;
参考文献
Gu, Wenxin; She, Xuegong; Pan, Xinfu; Yang, Teng-Kuei
Tetrahedron Asymmetry, 1998 , vol. 9, # 8 p. 1377 - 1380
反应条件
1: 4-bromo-phenol With sodium hydride in acetonitrile T=0 - 20°C; 0.333333 h; 2: chloromethyl methyl ether in acetonitrile T=20°C; 0.333333 h;
参考文献
Wyeth
Patent: US2005/282826 A1, 2005 ;
Location in patent: Page/Page column 21 ;
反应条件
phosphorus pentoxide in dichloromethane
参考文献
Diemer, Vincent; Chaumeil, Helene; Defoin, Albert; Fort, Alain; Boeglin, Alex; Carre, Christiane
European Journal of Organic Chemistry, 2006 , # 12 p. 2727 - 2738
反应条件
potassium carbonate in water; N,N-dimethyl-formamide
反应条件
N-bromosuccinmide; 2,2'-azo-bisisobutyronitrile in benzene 0.5 h; Heating;
参考文献
Livantsov, M. V.; Proskurnina, M. V.; Lutsenko, I. F.
J. Gen. Chem. USSR (Engl. Transl.), 1983 , vol. 53, # 5 p. 1032 - 1035,912 - 915
反应条件
sodium methylate 1.) DMF, rt, 30 min, 2.) DMF, rt, 10 min; Yield givenMultistep reaction;
参考文献
Synthetic Communications, , vol. 29, # 13 p. 2217 - 2223
反应条件
1: 1.) Mg / 1.) THF, 2.) THF, reflux, 3 h 2: 3N aq. HCl / tetrahydrofuran / 3 h / Heating View Scheme
参考文献
Gu, Wenxin; She, Xuegong; Pan, Xinfu; Yang, Teng-Kuei
Tetrahedron Asymmetry, 1998 , vol. 9, # 8 p. 1377 - 1380
反应条件
1: triethylamine; copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride / |Inert atmosphere; |Reflux 2: potassium hydroxide; potassium phosphate / toluene / |Inert atmosphere; |Reflux View Scheme
参考文献
Smeyanov, Alexey; Schmidt, Andreas
Synthetic Communications, 2013 , vol. 43, # 20 p. 2809 - 2816
反应条件
scandium tris(trifluoromethanesulfonate); Trimethylene glycol in acetonitrile T=50°C; 2 h;
参考文献
Synthetic Communications, , vol. 31, # 15 p. 2305 - 2311
