2-正戊丙烷-1,3-二醇合成路线 (共 12 条)
反应条件
sulfuric acid; hydrogen bromide
T=95 - 100°C; 18 h; Yield given;
参考文献
Haramoto; Nobe; Kamogawa
Bulletin of the Chemical Society of Japan, 1984 , vol. 57, # 7 p. 1966 - 1969
反应条件
1: 48percent HBr, conc. H2SO4 / 18 h / 95 - 100 °C
2: 1.) thiourea; 2.) tetraethylenepentamine / 1.) ethylene glycol, 75 deg C, 18 h; 2.) 75 deg C, 2 h
View Scheme
参考文献
Haramoto; Nobe; Kamogawa
Bulletin of the Chemical Society of Japan, 1984 , vol. 57, # 7 p. 1966 - 1969