1.1: 90 percent / aq. CAN / acetonitrile / 20 °C
2.1: HC(OMe)3 / methanol / 20 °C / pH 6
2.2: 77 percent / NaBH4 / methanol / 5 h / 0 °C
3.1: 54 percent / aq. CAN / acetonitrile; tetrahydrofuran / 20 °C
View Scheme
参考文献
Bull, Steven D.; Davies, Stephen G.; Fenton, Carry; Mulvaney, Andrew W.; Shyam Prasad; Smith, Andrew D.
Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 22 p. 3765 - 3774
1.1: HC(OMe)3 / methanol / 20 °C / pH 6
1.2: 77 percent / NaBH4 / methanol / 5 h / 0 °C
2.1: 54 percent / aq. CAN / acetonitrile; tetrahydrofuran / 20 °C
View Scheme
参考文献
Bull, Steven D.; Davies, Stephen G.; Fenton, Carry; Mulvaney, Andrew W.; Shyam Prasad; Smith, Andrew D.
Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 22 p. 3765 - 3774
Katritzky, Alan R.; Drewniak, Malgorzata
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 2339 - 2344