2,3-二苯基-1,3-丁二烯合成路线 （共 101 条）
反应条件
potassium hydrogensulfate; N-phenyl-N-β-naphthylamine
T=120°C; Dehydration; P=7 - 8 Torr; 0.666667 h;
参考文献
Niemi, Tuula-A.; Coe, Paul L.; Till, Stephen J.
Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 10 p. 1519 - 1528
反应条件
in tetrahydrofuran
Irradiation (UV/VIS); dissolving of the Mn compd., photolysing (Hanovia 450W) for 1.5 h, addn. of the dithiinoxide under N2 and stirring at 25°C for 2 h; rotary evapn., column chromy. (silica gel), elution with CH2Cl2-petroleum ether and recrystn. from CH2Cl2-petroleum ether;
参考文献
Urove, Greg A.; Welker, Mark E.
Organometallics, 1988 , vol. 7, p. 1013 - 1014
反应条件
tetrahydrofuran in tetrahydrofuran
characterization by spectroscopy and crystallography;
参考文献
Urove, Greg A.; Welker, Mark E.
Organometallics, 1988 , vol. 7, p. 1013 - 1014
反应条件
1: With samarium diiodide in tetrahydrofuran
0.25 h; Inert atmosphere;
2: With acetic anhydride in tetrahydrofuran
2.75 h; Reflux;
参考文献
Li, Jian; Li, Shaoyu; Jia, Xueshun
Synlett, 2008 , # 10 p. 1529 - 1531
反应条件
titanium tetrachloride; zinc in tetrahydrofuran
5 h; Heating;
参考文献
Nakayama, Juzo; Machida, Haruki; Hoshino, Masamatsu
Tetrahedron Letters, 1985 , vol. 26, # 16 p. 1981 - 1982
反应条件
η5-C5Me5Fe(CO)2CH3
T=100°C; 1.5 h;
参考文献
Powell, Kimberly R.; Elias, W. Jeff; Welker, Mark E.
Journal of Organometallic Chemistry, 1991 , vol. 407, # 1 p. 81 - 89
反应条件
in not given
identification by spectral comparison to an authentic sample;
参考文献
Urove, Greg A.; Welker, Mark E.; Eaton, Bruce E.
Journal of Organometallic Chemistry, 1990 , vol. 384, p. 105 - 114
反应条件
oxygen; palladium diacetate; p-benozquinone; lithium tert-butylate in dimethyl sulfoxide
T=90°C; P=760.051 Torr; 14 h; Molecular sieve; regioselective reaction;
参考文献
Jiang, Huanfeng; He, Li; Li, Xianwei; Chen, Huoji; Wu, Wanqing; Fu, Wei
Chemical Communications, 2013 , vol. 49, # 80 p. 9218 - 9220
反应条件
titanium tetrachloride; zinc in tetrahydrofuran
2 h; Heating;
参考文献
Nakayama, Juzo; Shibuya, Masahiro; Ikuina, Yoji; Murai, Fumito; Hoshino, Masamatsu
Phosphorus and Sulfur and the Related Elements, 1988 , vol. 38, p. 149 - 156
反应条件
in diethyl ether
T=0°C;
参考文献
Silva, Anthony N. De; Francis, Craig L.; Ward, A. David
Australian Journal of Chemistry, 1993 , vol. 46, # 11 p. 1657 - 1672
