2,3-二苯基-1,3-丁二烯合成路线 （共 101 条）
反应条件
1: 94 percent / m-chloroperbenzoic acid / CHCl3 / Ambient temperature
2: 90 percent / neat (no solvent) / 180 °C
View Scheme
参考文献
Nakayama, Juzo; Machida, Haruki; Saito, Ryuji; Akimoto, Keiichi; Hoshino, Masamatsu
Chemistry Letters, 1985 , p. 1173 - 1176
反应条件
Ca2+-montmorillonit in solid
T=160°C; 15 h; effects of homoionic-montmorillonits contains various metal ions; Product distribution;
参考文献
Gutierrez, Elvira; Ruiz-Hitzky, Eduardo
Molecular Crystals and Liquid Crystals (1969-1991), 1988 , vol. 161, p. 453 - 458
反应条件
1.1: Mg / diethyl ether / 0.67 h
1.2: 76 percent / diethyl ether / 4 h
2.1: 46 percent / KHSO4; phenyl-β-naphthylamine / 0.67 h / 120 °C / 7 - 8 Torr
View Scheme
参考文献
Niemi, Tuula-A.; Coe, Paul L.; Till, Stephen J.
Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 10 p. 1519 - 1528
反应条件
Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Takahashi; Xi; Fischer; Huo; Nakajima
Journal of the American Chemical Society, 1997 , vol. 119, # 19 p. 4561 - 4562
反应条件
in dichloromethane
under N2; dissolved org. S-compound was cooled to 0°C; addn. of BF3-Et2O; stirred for 0.25 h; dropwise addn. of Fe-complex soln.; stirred for 4 h at 0°C; addn. of H2O; extn. (CH2Cl2); dried (MgSO4); solvent removal by evapn.; chromy. (silica gel; eluent: CH2Cl2/petroleum ether);;
参考文献
Powell, Kimberly R.; Elias, W. Jeff; Welker, Mark E.
Journal of Organometallic Chemistry, 1991 , vol. 407, # 1 p. 81 - 89
反应条件
1: titanium tetrachloride; zinc
2: 1,2,4-trichloro-benzene / 6 h / Reflux
View Scheme
参考文献
Rys, Andrzej Z.; Schultz, Erwin K. V.; Harpp, David N.
Journal of Sulfur Chemistry, 2010 , vol. 31, # 5 p. 351 - 371
反应条件
in diethyl ether
1.) r.t., 30 min, 2.) reflux, 2 h;
参考文献
Silva, Anthony N. De; Francis, Craig L.; Ward, A. David
Australian Journal of Chemistry, 1993 , vol. 46, # 11 p. 1657 - 1672
反应条件
tetrakis(triphenylphosphine) palladium(0); magnesium
1.) THF, rerflux, 1 h, 2.) 1 h; Multistep reaction. Yields of byproduct given;
参考文献
Pasto, Daniel J.; Kong, Wei
Journal of Organic Chemistry, 1989 , vol. 54, # 17 p. 4028 - 4033
反应条件
1) CuCN*2LiBr
1) THF, -20 deg C, 15 min, 2) a) 0 deg C, 30 min, b) room temperature, 1 h; Yield given. Multistep reaction;
参考文献
Zhu, Lishan; Rieke, Reuben D.
Tetrahedron Letters, 1991 , vol. 32, # 25 p. 2865 - 2866
反应条件
Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Takahashi; Xi; Fischer; Huo; Nakajima
Journal of the American Chemical Society, 1997 , vol. 119, # 19 p. 4561 - 4562
