10,11,12,13-四氢苯并[b]苯并菲合成路线 (共 6 条)
反应条件
hydrogen; platinum on activated charcoal in ethyl acetate P=2068.6 Torr; 17 h; Ambient temperature;
参考文献
Fu, Peter P.; Lee, Hong M.; Harvey, Ronald G.
Journal of Organic Chemistry, 1980 , vol. 45, # 14 p. 2797 - 2803
反应条件
potassium hydroxide; hydrazine hydrate; diethylene glycol
参考文献
Buu-Hoi et al.
Journal of the Chemical Society, 1959 , p. 1845,1848
反应条件
1: SOCl2; pyridine; diethyl ether / Behandeln des Reaktionsprodukts mit AlCl3 in Nitrobenzol 2: N2H4+H2O; KOH; diethylene glycol View Scheme
参考文献
Buu-Hoi et al.
Journal of the Chemical Society, 1959 , p. 1845,1848
反应条件
1: N2H4+H2O; KOH 2: SOCl2; pyridine; diethyl ether / Behandeln des Reaktionsprodukts mit AlCl3 in Nitrobenzol 3: N2H4+H2O; KOH; diethylene glycol View Scheme
参考文献
Buu-Hoi et al.
Journal of the Chemical Society, 1959 , p. 1845,1848
反应条件
water; 2,3-dicyano-5,6-dichloro-p-benzoquinone in 1,4-dioxane 16 h; Heating;
参考文献
Lee, Hongmee; Harvey, Ronald G.
Journal of Organic Chemistry, 1983 , vol. 48, # 5 p. 749 - 751
反应条件
2,3-dicyano-5,6-dichloro-p-benzoquinone in benzene 0.166667 h; Heating; Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 45, # 1 p. 169 - 171