(R)-α-(氨基甲基)苄醇合成路线 (共 67 条)
反应条件
1.1: sodium ethanolate / ethanol / 0.17 h / 20 °C 1.2: 1 h / 0 °C 2.1: silver(l) oxide / dichloromethane / 0 - 20 °C 3.1: C10H18BNO; dimethylsulfide borane complex / tetrahydrofuran / 0 °C / Reflux 3.2: 5 h / 20 °C View Scheme
参考文献
Synthesis, , # 2 art. no. P14610SS, p. 316 - 324
反应条件
lithium aluminium tetrahydride in tetrahydrofuran 1 h; Heating; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Tetrahedron, , vol. 46, # 5 p. 1653 - 1658
反应条件
hydrogenchloride in methanol
参考文献
Bulletin of the Chemical Society of Japan, , vol. 66, # 4 p. 1216 - 1221
反应条件
hydrogenchloride in methanol
参考文献
Bulletin of the Chemical Society of Japan, , vol. 66, # 4 p. 1216 - 1221
反应条件
hydrogenchloride in methanol
参考文献
Bulletin of the Chemical Society of Japan, , vol. 66, # 4 p. 1216 - 1221
反应条件
1: H2O; ethanol / 504 h / 32 °C / baker's yeast, sucrose 2: 10percent aq. HCl / methanol View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 66, # 4 p. 1216 - 1221
反应条件
1: 84 percent / NaBH4 / ethanol / 6 h / 0 °C 3: 10percent aq. HCl / methanol View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 66, # 4 p. 1216 - 1221
反应条件
2: 10percent aq. HCl / methanol View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 66, # 4 p. 1216 - 1221
反应条件
2: 10percent aq. HCl / methanol View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 66, # 4 p. 1216 - 1221
反应条件
1: H2O; ethanol / 504 h / 32 °C / baker's yeast, sucrose 2: 10percent aq. HCl / methanol View Scheme
参考文献
Bulletin of the Chemical Society of Japan, , vol. 66, # 4 p. 1216 - 1221