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乙二醇
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63148-62-9
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二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
2549-35-1
合成路线
（共 14 条）
25755-94-6
2,5-二苯基-4-噁唑羧酸甲酯
→
反应条件
2549-35-1
反应条件
1: With lithium aluminium tetrahydride in tetrahydrofuran T=0°C; 0.166667 h; 2: With water in tetrahydrofuran T=0°C;
参考文献
Li, Ziyuan; Ma, Ling; Xu, Jinyi; Kong, Lingyi; Wu, Xiaoming; Yao, Hequan
Chemical Communications, 2012 , vol. 48, # 31 p. 3763 - 3765
93729-29-4
→
反应条件
2549-35-1
反应条件
lithium borohydride; lithium triethylborohydride in tetrahydrofuran
参考文献
McCairn, Mark C.; Culliford, Steven J.; Kozlowski, Roland Z.; Sutherland, Andrew J.
Tetrahedron Letters, 2004 , vol. 45, # 10 p. 2163 - 2166
92-71-7
2,5-二苯基恶唑
+
68-12-2
N,N-二甲基甲酰胺
→
反应条件
2549-35-1
反应条件
1: 2,5-diphenyl oxazole With sec.-butyllithium; [3H]-Thymidine monophosphate in tetrahydrofuran T=-75 - 0°C; 2: N,N-dimethyl-formamide T=20°C; 10 h; 3: With sodium tetrahydroborate in methanol
参考文献
McCairn, Mark C.; Culliford, Steven J.; Kozlowski, Roland Z.; Sutherland, Andrew J.
Tetrahedron Letters, 2004 , vol. 45, # 10 p. 2163 - 2166
59171-72-1
2-苯基噁唑-4-羧酸甲酯
→
反应条件
2549-35-1
反应条件
1.1: silver(I) acetate; palladium diacetate; 2,2,2-trimethylacetic acid / 12 h / 120 °C 2.1: lithium aluminium tetrahydride / tetrahydrofuran / 0.17 h / 0 °C 2.2: 0 °C View Scheme
参考文献
Li, Ziyuan; Ma, Ling; Xu, Jinyi; Kong, Lingyi; Wu, Xiaoming; Yao, Hequan
Chemical Communications, 2012 , vol. 48, # 31 p. 3763 - 3765
5333-86-8
苯甲亚胺酸乙酯盐酸盐
→
反应条件
2549-35-1
反应条件
1.1: triethylamine / dichloromethane / 0 - 20 °C 2.1: copper diacetate / N,N-dimethyl-formamide / 120 °C 3.1: silver(I) acetate; palladium dichloride; 2,2,2-trimethylacetic acid / 12 h / 120 °C 4.1: lithium aluminium tetrahydride / tetrahydrofuran / 0.17 h / 0 °C 4.2: 0 °C View Scheme
参考文献
Li, Ziyuan; Ma, Ling; Xu, Jinyi; Kong, Lingyi; Wu, Xiaoming; Yao, Hequan
Chemical Communications, 2012 , vol. 48, # 31 p. 3763 - 3765
100-52-7
苯甲醛
→
反应条件
2549-35-1
反应条件
1.1: hydroxylamine hydrochloride; sodium carbonate / methanol; water / Reflux 2.1: acetic anhydride / Reflux 3.1: hydrogenchloride / 0 - 20 °C 4.1: triethylamine / dichloromethane / 0 - 20 °C 5.1: copper diacetate / N,N-dimethyl-formamide / 120 °C 6.1: silver(I) acetate; palladium dichloride; 2,2,2-trimethylacetic acid / 12 h / 120 °C 7.1: lithium aluminium tetrahydride / tetrahydrofuran / 0.17 h / 0 °C 7.2: 0 °C View Scheme
参考文献
Bodendorf,K.; Towliati,H.
Archiv der Pharmazie und Berichte der Deutschen Pharmazeutischen Gesellschaft, 1965 , vol. 298, p. 293 - 297
100-47-0
苯甲腈
→
反应条件
2549-35-1
反应条件
1.1: hydrogenchloride / 0 - 20 °C 2.1: triethylamine / dichloromethane / 0 - 20 °C 3.1: copper diacetate / N,N-dimethyl-formamide / 120 °C 4.1: silver(I) acetate; palladium dichloride; 2,2,2-trimethylacetic acid / 12 h / 120 °C 5.1: lithium aluminium tetrahydride / tetrahydrofuran / 0.17 h / 0 °C 5.2: 0 °C View Scheme
参考文献
Li, Ziyuan; Ma, Ling; Xu, Jinyi; Kong, Lingyi; Wu, Xiaoming; Yao, Hequan
Chemical Communications, 2012 , vol. 48, # 31 p. 3763 - 3765
932-90-1
苯甲醛肟
→
反应条件
2549-35-1
反应条件
1.1: acetic anhydride / Reflux 2.1: hydrogenchloride / 0 - 20 °C 3.1: triethylamine / dichloromethane / 0 - 20 °C 4.1: copper diacetate / N,N-dimethyl-formamide / 120 °C 5.1: silver(I) acetate; palladium dichloride; 2,2,2-trimethylacetic acid / 12 h / 120 °C 6.1: lithium aluminium tetrahydride / tetrahydrofuran / 0.17 h / 0 °C 6.2: 0 °C View Scheme
参考文献
Li, Ziyuan; Ma, Ling; Xu, Jinyi; Kong, Lingyi; Wu, Xiaoming; Yao, Hequan
Chemical Communications, 2012 , vol. 48, # 31 p. 3763 - 3765
55044-06-9
→
反应条件
2549-35-1
反应条件
1.1: copper diacetate / N,N-dimethyl-formamide / 120 °C 2.1: silver(I) acetate; palladium dichloride; 2,2,2-trimethylacetic acid / 12 h / 120 °C 3.1: lithium aluminium tetrahydride / tetrahydrofuran / 0.17 h / 0 °C 3.2: 0 °C View Scheme
参考文献
Li, Ziyuan; Ma, Ling; Xu, Jinyi; Kong, Lingyi; Wu, Xiaoming; Yao, Hequan
Chemical Communications, 2012 , vol. 48, # 31 p. 3763 - 3765
2549-33-9
→
反应条件
2549-35-1
反应条件
sodium hydroxide in ethanol
参考文献
Bodendorf,K.; Towliati,H.
Archiv der Pharmazie und Berichte der Deutschen Pharmazeutischen Gesellschaft, 1965 , vol. 298, p. 293 - 297
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