反应条件
1.1: 49 percent / CuCN*2LiCl / tetrahydrofuran; dimethylformamide / -30 - 20 °C 2.1: 97 percent / Et3N; DMAP 3.1: 97 percent / DIBAL-H / tetrahydrofuran; toluene / 1 h / -78 °C 4.1: 25 percent / formic acid / 0.17 h / 0 - 20 °C 5.1: ozone / CH2Cl2 / 0.17 h / -78 °C 5.2: 93 percent / dimethyl sulfide / CH2Cl2 / 2 h / 20 °C View Scheme
参考文献
Karstens, Willem F. J.; Moolenaar, Marinus J.; Rutjes, Floris P. J. T.; Grabowska, Urszula; Speckamp, W. Nico; Hiemstra, Henk
Tetrahedron Letters, 1999 , vol. 40, # 49 p. 8629 - 8632
