1,4-苯并二氧杂环己烷合成路线 （共 15 条）
参考文献
Moureu
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1899 , vol. 128, p. 559
Bulletin de la Societe Chimique de France, 1899 , vol. <3> 21, p. 295
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Moureu
Annales de Chimie (Cachan, France), 1899 , vol. <7> 18, p. 130
反应条件
ozone; trifluoroacetic acid 1.) CH2Cl2, -78 deg C, 2.) CH2Cl2, -78 deg C, 3 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Kashima, Choji; Tomotake, Atsushi; Omote, Yoshimori
Journal of Organic Chemistry, 1987 , vol. 52, # 25 p. 5616 - 5621
反应条件
ozone 1.) CH2Cl2, -78 deg C, 2.) CH2Cl2, -78 deg C, irradiation; Yield given. Multistep reaction;
参考文献
Kashima, Choji; Tomotake, Atsushi; Omote, Yoshimori
Heterocycles, 1987 , vol. 26, # 2 p. 363 - 366
反应条件
ozone; trifluoroacetic acid 1.) CH2Cl2, -78 deg C, 2.) CH2Cl2, -78 deg C, 3 h; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Kashima, Choji; Tomotake, Atsushi; Omote, Yoshimori
Journal of Organic Chemistry, 1987 , vol. 52, # 25 p. 5616 - 5621
反应条件
1: 1) n-BuLi / 1) in THF, hexane, -78 deg C, 1h, 2) RT, 8h 2: 1) n-BuLi / 1) in THF, hexane, -78 deg C, 1h, 2) RT, 8h 3: 33 percent / O2, Rose Bengal / CH2Cl2 / 2 h / -78 °C / Irradiation 4: xylene / 97 °C / ΔH(excit.), ΔS(excit.), ΔG(excit.), other temp., chemiluminescence technique (DBA) View Scheme
参考文献
Adam, Waldemar; Peters, Eva-Maria; Peters, Karl; Platsch, Herbert; Schmidt, Ernst; et al.
Journal of Organic Chemistry, 1984 , vol. 49, # 21 p. 3920 - 3928
