3-甲基-4-苯基-2-丁酮合成路线 （共 34 条）
反应条件
2-Chloro-2-methylpropane; sodium iodide in acetonitrile 24 h; Heating;
参考文献
Sakai, Takashi; Miyata, Kazuyoshi; Hondo, Kazuomi; Utaka, Masanori; Takeda, Akira
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 9 p. 3421 - 3422
反应条件
water; [Rh(NCMe)2(cod)][BF4] in tetrahydrofuran T=60°C; 5 h;
参考文献
Oi, Shuichi; Moro, Mitsutoshi; Ito, Hisanori; Honma, Yoshio; Miyano, Sotaro; Inoue, Yoshio
Tetrahedron, 2002 , vol. 58, # 1 p. 91 - 97
反应条件
in diethyl ether T=0 - 20°C; 3.16667 h;
参考文献
SEPRACOR INC.
Patent: US2005/143443 A1, 2005 ;
Location in patent: Page/Page column 27-28 ;
反应条件
1: Methyltriphenylphosphonium bromide With n-butyllithium in tetrahydrofuran; hexane T=-15°C; 2: N-methoxy-N-methyl-α-methylhydrocinnamamide in tetrahydrofuran; hexane T=-78 - 20°C; Wittig reaction; 3: With hydrogenchloride in tetrahydrofuran; diethyl ether; hexane T=20°C;
参考文献
Murphy, John A.; Commeureuc, Aurelien G. J.; Snaddon, Thomas N.; McGuire, Thomas M.; Khan, Tanweer A.; Hisler, Kevin; Dewis, Mark L.; Carling, Robert
Organic Letters, 2005 , vol. 7, # 7 p. 1427 - 1429
反应条件
tetrabutylammomium bromide; sodium hydrogencarbonate; palladium dichloride T=120°C; Heck coupling; 24 h;
参考文献
Bouquillon, Sandrine; Ganchegui, Benjamin; Estrine, Boris; Henin, Francoise; Muzart, Jacques
Journal of Organometallic Chemistry, 2001 , vol. 634, # 2 p. 153 - 156
反应条件
tetrabutylammomium bromide; sodium hydrogencarbonate; palladium dichloride T=120°C; Heck coupling; 4 h;
参考文献
Bouquillon, Sandrine; Ganchegui, Benjamin; Estrine, Boris; Henin, Francoise; Muzart, Jacques
Journal of Organometallic Chemistry, 2001 , vol. 634, # 2 p. 153 - 156
反应条件
(NH4)2S2O8; [{(η5-C5Me5)RhCl}2(μ-Cl)2] in water T=110°C; 12 h; Inert atmosphereSealed tube;
参考文献
Organic Letters, , vol. 16, # 1 p. 66 - 69
反应条件
in tetrahydrofuran; diethyl ether T=0°C; 2.5 h;
参考文献
Martin; Romea; Tey; Urpi; Vilarrasa
Synlett, 1997 , # 12 p. 1414 - 1416
反应条件
T=160 - 200°C; P=0.05 Torr;
参考文献
Ahmar; Bloch; Bortolussi
Synthetic Communications, 1991 , vol. 21, # 8-9 p. 1071 - 1074
反应条件
H2 activated rhodium-phosphinine complex in 1,4-dioxane T=60°C; 2 h;
参考文献
Synlett, , # 13 p. 2127 - 2129
