3-甲基-4-苯基-2-丁酮合成路线 (共 34 条)
反应条件
chloro-trimethyl-silane; sodium iodide in acetonitrile 6 h, room temperature, then 10 h , 60 deg C;
参考文献
Sakai; Miyata; Tsuboi; Utaka
Bulletin of the Chemical Society of Japan, 1989 , vol. 62, # 12 p. 4072 - 4074
反应条件
tert.-butylhydroperoxide; C96H98Fe2N17 in water T=60°C; P=1500.15 - 2250.23 Torr; 24 h; Inert atmosphere;
参考文献
Chemistry - A European Journal, , vol. 17, # 34 p. 9298 - 9301
反应条件
in N,N,N',N',N'',N''-hexamethylphosphoric triamide T=40°C; 4 h;
参考文献
Shibata, Ikuya; Nishio, Masahiro; Baba, Akio; Matsuda, Haruo
Chemistry Letters, 1993 , # 11 p. 1953 - 1956
反应条件
potassium tetrachloroplatinate(II); potassium hydroxide in 1,4-dioxane; water 2 h; HeatingInert atmosphere;
参考文献
Watanabe, Eiichi; Kaiho, Atsushi; Kusama, Hiroyuki; Iwasawa, Nobuharu
Journal of the American Chemical Society, 2013 , vol. 135, # 32 p. 11744 - 11747
反应条件
ammonia; lithium in tert-butyl alcohol
参考文献
Journal of Organic Chemistry, , vol. 35, p. 1881 - 1886
反应条件
chloro-trimethyl-silane; water; sodium iodide in hexane 31 h; Ambient temperature;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 60, # 3 p. 1063 - 1066
反应条件
1.1: 100 percent / tetrahydrofuran / -78 °C 2.1: n-BuLi / tetrahydrofuran; hexane / -15 °C 2.2: tetrahydrofuran; hexane / -78 - 20 °C 2.3: 75 percent / aq. HCl / tetrahydrofuran; hexane; diethyl ether / 20 °C View Scheme
参考文献
Organic Letters, , vol. 7, # 7 p. 1427 - 1429
反应条件
1: With copper(l) iodide; potassium carbonate; N,N'-dimethylcyclohexane-1,2-diamine in tetrahydrofuran 2: With water in tetrahydrofuran
参考文献
Organic Letters, , vol. 11, # 18 p. 4084 - 4087
反应条件
DEMS; bis(1,2-diphenylphosphino)benzene; copper (II) acetate monohydrate in tetrahydrofuran T=20°C; 10 h; Inert atmosphere;
参考文献
Journal of the American Chemical Society, , vol. 132, # 23 p. 7852 - 7853
反应条件
DEMS; (RP,R)-Taniaphos; copper (II) acetate monohydrate in tetrahydrofuran T=20°C; 4.5 h; Inert atmosphere; optical yield given as percent eeenantioselective reaction;
参考文献
Moser, Ralph; Boskovia, Zarko V.; Crowe, Christopher S.; Lipshutz, Bruce H.
Journal of the American Chemical Society, 2010 , vol. 132, # 23 p. 7852 - 7853