3-甲基-4-苯基-2-丁酮合成路线 （共 34 条）
反应条件
1: concentrated aqueous hydrochloric acid 2: ethanol; Raney nickel / 50 - 60 °C / 40452.9 Torr / Hydrogenation View Scheme
参考文献
Annales de Chimie (Cachan, France), , vol. <12>4, p. 242
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, , vol. 226, p. 500
反应条件
hydrogenchloride; TiCl3; sodium nitrite 1.) 0-5 degC, 2.) Acetone, 30 min, 40 degC;
参考文献
Citterio, Attilio; Vismara, Elena
Synthesis, 1980 , # 4 p. 291 - 292
反应条件
[{(η5-C5Me5)RhCl}2(μ-Cl)2]; sodium formate; N-(2-amino-ethyl)-4-methyl-benzenesulphonamide; sodium hydroxide in water T=60°C; 38 h; Inert atmosphere; chemoselective reaction;
参考文献
Journal of Organic Chemistry, , vol. 75, # 9 p. 2981 - 2988
反应条件
1: porcine liver acetone powder (PLAP), 2N aq. NaOH / H2O / 21 h / 20 °C / pH 7.2 2: 82 percent / 160 - 200 °C / 0.05 Torr View Scheme
参考文献
Synthetic Communications, , vol. 21, # 8-9 p. 1071 - 1074
反应条件
aluminium trichloride T=10 - 20°C;
参考文献
Bulletin de la Societe Chimique de France, , p. 177,183
反应条件
dichloro(.eta.3:.eta.2:.eta.3-dodeca-2,6,10-triene-1,12-diyl)ruthenium(IV); water; sodium formate T=100°C; 20 h; Inert atmosphere;
参考文献
Green Chemistry, , vol. 11, # 12 p. 1992 - 2000
反应条件
water; lithium 1.) THF, RT, 2.) THF, 1.5 h; Yield given. Multistep reaction;
参考文献
Journal of Organic Chemistry, , vol. 53, # 8 p. 1741 - 1744
反应条件
FcSO2-cyclo[-N(CH2CH=CHCH2N(Ts))2CH2CH=CHCH2-]Pd(O) in ethanol T=20°C; Heck arylation; 4.25 h; Product distribution; Further Variations:CatalystsSolventsTemperaturesreactant ratio, reaction times;
参考文献
Journal of Organometallic Chemistry, , vol. 690, # 16 p. 3822 - 3826
反应条件
trifluoroacetic acid
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 2263 - 2272
反应条件
(i) nBuLi, THF, hexane, (ii) /BRN= 969135/, (iii) /BRN= 471308/; Multistep reaction;
参考文献
Journal of Organic Chemistry, , vol. 41, # 3 p. 439 - 442
