反应条件
in N,N-dimethyl-formamide
Stirring of mixt. of TBAFe and 3-chloro-2-methylsiloxy-1-propene in DMF at room temp. for 2 h, addn. of 2-propynyl bromide, heating (80°C, 15 h).; Hydrolizing (aq. HCl), extg. (ether), washing of ext. (H2O), drying (Na2SO4), evapn. in vac., chromy. (silica gel, hexane-ethyl acetate), elem. anal.;
参考文献
Itoh, Keiji; Nakanishi, Saburo; Otsuji, Yoshio
Bulletin of the Chemical Society of Japan, 1991 , vol. 64, # 10 p. 2965 - 2977
