ammonium acetate in benzene

1: 82 percent / potassium hydroxide / methanol / 8 h / steam distillation 2: 1) HCl, aluminium chloride 2) aqueous H2SO4 / 1) tetrachloroethane, 8 h, 65-70 deg C 2) overnight, room temperature 3) steam distillation 3: 1) KOH 2) acetic anhydride, sodium acetate / 1) ethanol, water, 5 deg C, 2 days 2) reflux, 20 min. View Scheme

1: 1) HCl, aluminium chloride 2) aqueous H2SO4 / 1) tetrachloroethane, 8 h, 65-70 deg C 2) overnight, room temperature 3) steam distillation 2: 1) KOH 2) acetic anhydride, sodium acetate / 1) ethanol, water, 5 deg C, 2 days 2) reflux, 20 min. View Scheme

lithium aluminium tetrahydride in tetrahydrofuran