1,3-二(苄氧基羰基)-2-甲基异硫代脲合成路线 (共 6 条)
反应条件
in dichloromethane; water; sodium hydrogencarbonate T=20°C; 25 h;
参考文献
CENTRE NATIONAL DE LA RECHERCHE SCIENTIFIQUE (C.N.
Patent: US2005/176819 A1, 2005 ;
Location in patent: Page/Page column 6 ;
反应条件
sodium hydroxide; sodium hydrogencarbonate in dichloromethane T=0°C; 3 h;
参考文献
Lal, Bansi; Gangopadhyay
Tetrahedron Letters, 1996 , vol. 37, # 14 p. 2483 - 2486
反应条件
sodium hydroxide in 1,4-dioxane 18 h;
参考文献
Gers, Tomasz; Kunce, Danuta; Markowski, Pawel; Izdebski, Jan
Synthesis, 2004 , # 1 p. 37 - 42
反应条件
sodium hydroxide in 1,4-dioxane 48 h;
参考文献
Gers, Tomasz; Kunce, Danuta; Markowski, Pawel; Izdebski, Jan
Synthesis, 2004 , # 1 p. 37 - 42
反应条件
ammonia in methanol T=20°C; 3 h; Inert atmosphere;
参考文献
Limbach, Michael; Korotkov, Vadim S.; Es-Sayed, Mazen; De Meijere, Armin
Organic and Biomolecular Chemistry, 2008 , vol. 6, # 20 p. 3816 - 3822
反应条件
1.2: 20 °C 2.1: hydrogenchloride / ethyl acetate 3.1: 4-methyl-morpholine / tetrahydrofuran / 20 °C View Scheme
参考文献
Yuan, Jian Hai; Yang, Xiao Xiao; Lin, Hao; Wang, De Xin
Chinese Chemical Letters, 2011 , vol. 22, # 12 p. 1399 - 1402