三乙基-[2-[4-[(E)-2-苯乙烯基]苯氧基]乙基]铵碘化物合成路线 （共 4 条）
反应条件
1: 1.) BuLi, 2.) ZnCl2, 3.) tetrakis (triphenylphosphine)palladium / 1.) ether, hexane, -78 deg C, 1h; -78 deg C - room temperature, 2.) THF, room temperature, 1 h, 3.) reflux, 24 h 2: i-Bu2AlH / benzene; hexane / 1.) room temperature, 0.5 h, 2.) reflux, 6 h 3: tetrahydrofuran / 1 h View Scheme
参考文献
Al-Hassan, Mohammed I.
Synthetic Communications, 1989 , vol. 19, # 9-10 p. 1677 - 1680
反应条件
1: i-Bu2AlH / benzene; hexane / 1.) room temperature, 0.5 h, 2.) reflux, 6 h 2: tetrahydrofuran / 1 h View Scheme
参考文献
Al-Hassan, Mohammed I.
Synthetic Communications, 1989 , vol. 19, # 9-10 p. 1677 - 1680
反应条件
1: 1.) BuLi, 2.) ZnCl2, 3.) tetrakis (triphenylphosphine)palladium / 1.) ether, hexane, -78 deg C, 1h; -78 deg C - room temperature, 2.) THF, room temperature, 1 h, 3.) reflux, 24 h 2: i-Bu2AlH / benzene; hexane / 1.) room temperature, 0.5 h, 2.) reflux, 6 h 3: tetrahydrofuran / 1 h View Scheme
参考文献
Al-Hassan, Mohammed I.
Synthetic Communications, 1989 , vol. 19, # 9-10 p. 1677 - 1680
反应条件
in tetrahydrofuran 1 h; Yield given;
参考文献
Al-Hassan, Mohammed I.
Synthetic Communications, 1989 , vol. 19, # 9-10 p. 1677 - 1680
