3-甲基-2-喹喔啉甲醛合成路线 （共 13 条）
反应条件
1: With diisobutylaluminium hydride in tetrahydrofuran; toluene T=-78°C; 2: With methanol in tetrahydrofuran; toluene T=-78°C;
参考文献
MITSUBISHI TANABE PHARMA CORPORATION; MORIMOTO, Hiroshi; SAKAMOTO, Toshiaki; HIMIYAMA, Toshiyuki; KAWANISHI, Eiji; MATSUMURA, Takehiko
Patent: WO2010/30027 A1, 2010 ;
Location in patent: Page/Page column 58; 59 ;
WO 2010/030027 A1
参考文献
TOPOTARGET UK LIMITED
Patent: WO2004/76386 A2, 2004 ;
Location in patent: Page 99 ;
反应条件
2-Nitropropane; sodium methylate in methanol T=20°C; 4 h;
参考文献
Chen, Yu-Jen; Hung, Hao-Chih; Sha, Chin-Kang; Chung, Wen-Sheng
Tetrahedron, 2010 , vol. 66, # 1 p. 176 - 182
反应条件
sodium periodate; sodium hydrogencarbonate in water Ambient temperature;
参考文献
Beck, Jakob; Ledl, Franz; Severin, Theodor
Carbohydrate Research, 1988 , vol. 177, p. 240 - 243
反应条件
hydrogenchloride 0.166667 h;
参考文献
Vogel, M.; Lippmann, E.
Journal fuer Praktische Chemie (Leipzig), 1987 , vol. 329, # 1 p. 101 - 107
反应条件
1: 70 percent / phosphate buffer (pH 7) / 10 h / Heating 2: 73 percent / sodium periodate, sodium hydrogencarbonate / H2O / Ambient temperature View Scheme
参考文献
Carbohydrate Research, , vol. 177, p. 240 - 243
反应条件
1: 69 percent / K2CO3 / methanol; H2O / 0.5 h 2: 84 percent / 2 n HCl / 0.17 h View Scheme
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. 329, # 1 p. 101 - 107
反应条件
selenium(IV) oxide; m-xylene
参考文献
Chemische Berichte, , vol. 84, p. 477
参考文献
Chemische Berichte, , vol. 84, p. 477
反应条件
potassium permanganate; sulfuric acid in pyridine; water 24 h;
参考文献
Kepez, Mustafa
Monatshefte fuer Chemie, 1989 , vol. 120, p. 127 - 130
