3-(苄氧基)异噁唑-5-甲醛合成路线 （共 6 条）
反应条件
dipyridinium dichromate in dichloromethane T=20°C; 16 h;
参考文献
ABBOTT LABORATORIES; ABBOTT GMBH and CO.KG; MARING, Clarence J.; PRATT, John K.; CARROLL, William A.; LIU, Dachun; BETEBENNER, David A.; HUTCHINSON, Douglas K.; TUFANO, Michael D.; ROCKWAY, Todd W.; SCHOEN, Uwe; PAHL, Axel; WITTE, Adreas
Patent: WO2012/87833 A1, 2012 ;
Location in patent: Page/Page column 133 ;
WO 2012/087833 A1
反应条件
diisobutylaluminium hydride in hexane; dichloromethane T=-78°C; 1 h;
参考文献
Riess, Regine; Schoen, Michael; Laschat, Sabine; Jaeger, Volker
European Journal of Organic Chemistry, 1998 , # 3 p. 473 - 479
反应条件
1: 93 percent / K2CO3 / acetone / 3 h / 70 °C 2: 98 percent / DIBAH / CH2Cl2; hexane / 1 h / -78 °C View Scheme
参考文献
European Journal of Organic Chemistry, , # 3 p. 473 - 479
反应条件
in acetic acid T=80°C; 10 h;
参考文献
Chemical and pharmaceutical bulletin, , vol. 15, # 7 p. 1025 - 1031
反应条件
lithium aluminium tetrahydride
参考文献
Tetrahedron Letters, , p. 2081 - 2084
反应条件
1: aq. KOH / 2 h / 140 °C 2: LiAlH4 View Scheme
参考文献
Tetrahedron Letters, , p. 2081 - 2084
