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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
2-甲氧基苯甲酮
合成路线
（共 78 条）
5720-06-9
2-甲氧基苯基硼酸
+
100-52-7
苯甲醛
→
反应条件
2553-04-0
2-甲氧基苯甲酮
反应条件
potassium phosphate; 3,3-dimethyl-butan-2-one; C14H10Cl2N2O2Ru; [(t-Bu)3PH]BF4 in water; toluene T=100°C; 24 h;
参考文献
Dey, Bikash Kali; Dutta, Jayita; Drew, Michael G.B.; Bhattacharya, Samaresh
Journal of Organometallic Chemistry, 2014 , vol. 750, p. 176 - 184
5720-06-9
2-甲氧基苯基硼酸
+
98-88-4
苯甲酰氯
→
反应条件
2553-04-0
2-甲氧基苯甲酮
反应条件
copper(I) thiophene-2-carboxylate; triphenylphosphine; bis(dibenzylideneacetone)-palladium(0) in diethyl ether T=20°C; 3 h;
参考文献
Ogawa, Daisuke; Hyodo, Keita; Suetsugu, Masato; Li, Jing; Inoue, Yoshiaki; Fujisawa, Mamoru; Iwasaki, Masayuki; Takagi, Kentaro; Nishihara, Yasushi
Tetrahedron, 2013 , vol. 69, # 12 p. 2565 - 2571
578-57-4
2-溴苯甲醚
+
63468-90-6
→
反应条件
2553-04-0
2-甲氧基苯甲酮
反应条件
quinoline; 1,10-phenanthroline; tris-(o-tolyl)phosphine; copper(I) bromide in 1-methyl-pyrrolidin-2-one; quinoline T=170°C; 16 h;
参考文献
Goossen, Lukas J.; Rudolphi, Felix; Oppel, Christoph; Rodriguez, Nuria
Angewandte Chemie - International Edition, 2008 , vol. 47, # 16 p. 3043 - 3045
529-28-2
2-碘苯甲醚
+
201230-82-2
+
98-80-6
苯硼酸
→
反应条件
2553-04-0
2-甲氧基苯甲酮
反应条件
10 palladium on activated carbon; potassium carbonate in methoxybenzene T=100°C; Suzuki carbonylation; P=10343.2 Torr; 8 h; Autoclave;
参考文献
Khedkar, Mayur V.; Tambade, Pawan J.; Qureshi, Ziyauddin S.; Bhanage, Bhalchandra M.
European Journal of Organic Chemistry, 2010 , # 36 p. 6981 - 6986
681-84-5
正硅酸甲酯
+
16463-33-5
→
反应条件
2553-04-0
2-甲氧基苯甲酮
+
6136-67-0
3-乙氧基二苯甲酮
反应条件
oxygen; copper diacetate; silver carbonate in N,N-dimethyl-formamide T=145°C; 18 h;
参考文献
Journal of the American Chemical Society, , vol. 134, # 24 p. 9938 - 9941
591-50-4
碘苯
+
201230-82-2
+
5720-06-9
2-甲氧基苯基硼酸
→
反应条件
2553-04-0
2-甲氧基苯甲酮
反应条件
1: iodobenzene; 2-Methoxyphenyl-dihydroxyborane With potassium carbonate in toluene Suzuki cross-coupling reaction; 0.166667 h; Autoclave; 2: carbon monoxide in toluene T=100°C; Suzuki cross-coupling reaction; P=5171.62 Torr; 10 h; Autoclave;
参考文献
Qureshi, Ziyauddin S.; Deshmukh, Krishna M.; Tambade, Pawan J.; Bhanage, Bhalchandra M.
Synthesis, 2011 , # 2 art. no. P15410SS, p. 243 - 250
579-75-9
邻甲氧基苯甲酸
+
98-80-6
苯硼酸
→
反应条件
2553-04-0
2-甲氧基苯甲酮
反应条件
1: ortho-methoxybenzoic acid With potassium phosphate in 1,4-dioxane T=20°C; 0.0833333 h; Inert atmosphere; 2: With DMEG in 1,4-dioxane T=20°C; 2 h; Inert atmosphere; 3: 3,4,5-trimethoxyphenylboronic acid With tetrakis(triphenylphosphine) palladium(0) in 1,4-dioxane T=90°C; 16 h; Inert atmosphereSealed tube;
参考文献
Pathak, Arunendra; Rajput, Chatrasal S.; Bora, Pushkar S.; Sharma, Somesh
Tetrahedron Letters, 2013 , vol. 54, # 17 p. 2149 - 2150
5720-06-9
2-甲氧基苯基硼酸
+
318257-78-2
→
反应条件
2553-04-0
2-甲氧基苯甲酮
反应条件
tris(dibenzylideneacetone)dipalladium(0) chloroform complex; copper(I) thiophene-2-carboxylate; trifuran-2-yl-phosphane in tetrahydrofuran T=50°C; 18 h;
参考文献
Liebeskind; Srogl
Journal of the American Chemical Society, 2000 , vol. 122, # 45 p. 11260 - 11261
135-02-4
2-甲氧基苯甲醛
→
反应条件
2553-04-0
2-甲氧基苯甲酮
反应条件
[Rh(C2H4)2Cl]2; tri-tert-butyl phosphine in 1,4-dioxane; acetone T=80°C;
参考文献
Pucheault, Mathieu; Darses, Sylvain; Genet, Jean-Pierre
Journal of the American Chemical Society, 2004 , vol. 126, # 47 p. 15356 - 15357
17264-78-7
+
23665-09-0
苯基碘化锌
→
反应条件
2553-04-0
2-甲氧基苯甲酮
反应条件
1: sodium orthomethoxy benzoate With chloroformic acid ethyl ester in tetrahydrofuran T=20°C; 0.25 h; 2: Ph–ZnI With tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran T=70°C; Negishi-type cross-coupling; 14 h;
参考文献
Wang, Donghui; Zhang, Zhaoguo
Organic Letters, 2003 , vol. 5, # 24 p. 4645 - 4648
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