3,5-二甲基苯基苯基醚合成路线 （共 11 条）
反应条件
copper(l) iodide; iron (III) acetylacetonate; potassium carbonate in N,N-dimethyl-formamide T=135°C; 12 h; Inert atmosphere;
参考文献
Liu, Xiaoyan; Zhang, Songlin
Synlett, 2011 , # 2 art. no. W15810ST, p. 268 - 272
反应条件
methyl pyridin-2-ylmethyl ketone; caesium carbonate; copper(I) bromide in dimethyl sulfoxide T=80°C; 7 h; Inert atmosphere; chemoselective reaction;
参考文献
Zhang, Qi; Wang, Deping; Wang, Xianyang; Ding, Ke
Journal of Organic Chemistry, 2009 , vol. 74, # 18 p. 7187 - 7190
反应条件
copper(l) iodide; caesium carbonate in isobutyl methylketone T=110°C; Ullmann type condensation; 24 h; Inert atmosphere;
参考文献
Benyahya, Sofia; Monnier, Florian; Wong Chi Man, Michel; Bied, Catherine; Ouazzani, Fouad; Taillefer, Marc
Green Chemistry, 2009 , vol. 11, # 8 p. 1121 - 1123
反应条件
caesium carbonate; copper(I) oxide; trans-1,2-bis(2'-pyridylideneamino)cyclohexane in acetonitrile T=82°C; 24 h; activated 3 A molecular sieve (KnNa12-n[(AlO2)12(SiO2)12]); Conversion of starting material;
参考文献
Cellier, Pascal Philippe; Cristau, Henri-Jean; Spindler, Jean-Francis; Taillefer, Marc
Patent: US2003/236413 A1, 2003 ;
Location in patent: Page 31 ;
反应条件
2,2,6,6-tetramethylheptane-3,5-dione; caesium carbonate; copper(I) bromide in N,N-dimethyl-formamide T=135°C; 36 h; Inert atmosphere;
参考文献
CENTRE NATIONAL DE LA RECHERCHE SCIENTIFIQUE (C.N.R.S)
Patent: US2011/306782 A1, 2011 ;
Location in patent: Page/Page column 13 ;
反应条件
potassium tert-butylate in tert-butyl alcohol T=20°C; 20 h;
参考文献
Ozanne-Beaudenon, Aurelie; Quideau, Stephane
Angewandte Chemie - International Edition, 2005 , vol. 44, # 43 p. 7065 - 7069
反应条件
Cu(II) pivalate in dichloromethane T=25°C; 24 h;
参考文献
Rasmussen, L. Kyhn; Begtrup, Mikael; Ruhland, Thomas
Journal of Organic Chemistry, 2004 , vol. 69, # 20 p. 6890 - 6893
反应条件
copper diacetate; triethylamine in dichloromethane T=50°C; 3 h; Sealed tube;
参考文献
Crifar, Cynthia; Petiot, Pauline; Ahmad, Tabinda; Gagnon, Alexandre
Chemistry - A European Journal, 2014 , vol. 20, # 10 p. 2755 - 2760
反应条件
pyridine; copper diacetate in dichloromethane 18 h; Molecular sieve;
参考文献
Johnson, Steven M.; Connelly, Stephen; Wilson, Ian A.; Kelly, Jeffery W.
Journal of Medicinal Chemistry, 2008 , vol. 51, # 20 p. 6348 - 6358
反应条件
potassium carbonate in dimethyl sulfoxide 0.133333 h; RefluxMicrowave irradiation;
参考文献
Sarkate, Aniket P.; Bahekar, Sushilkumar S.; Wadhai, Vijay M.; Ghandge, Ganesh N.; Wakte, Pravin S.; Shinde, Devanand B.
Synlett, 2013 , vol. 24, # 12 art. no. ST-2013-B0227-L, p. 1513 - 1516
