N-2,2-丙烯基-2-丙烯酰胺合成路线 （共 7 条）
反应条件
1: 1-amino-2-propene With triethylamine in dichloromethane T=-78°C; Inert atmosphere; 2: acryloyl chloride in dichloromethane T=-78 - 20°C; 24 h; Inert atmosphere;
参考文献
Petersen, Mette T.; Nielsen, Thomas E.
Organic Letters, 2013 , vol. 15, # 8 p. 1986 - 1989
反应条件
potassium carbonate T=20°C; 18 h; Inert atmosphere;
参考文献
Petersen, Mette T.; Nielsen, Thomas E.
Organic Letters, 2013 , vol. 15, # 8 p. 1986 - 1989
反应条件
Tl(OCOCF3)3 1.) -20 deg C, 1 h, 2.) 0 deg C, 2 h;
参考文献
Ochiai, Masahito; Tada, Shin-Ichi; Arimoto, Masao; Fujita, Eiichi
Chemical and Pharmaceutical Bulletin, 1982 , vol. 30, # 8 p. 2836 - 2839
反应条件
carbon monoxide; tetracarbonylnickel(0); toluene
参考文献
Rohm and Haas Co.
Patent: US2773063 , 1954 ;
反应条件
copper diacetate in water; acetone
T=5 - 10°C; Arylation;
参考文献
Grishchuk; Klimnyuk; Zagrichuk; Kravchenyuk; Kolomiets; Gorbovoi
Pharmaceutical Chemistry Journal, 1999 , vol. 33, # 3 p. 143 - 144
反应条件
copper diacetate in water; acetone
T=5 - 10°C; Arylation; 3 h;
参考文献
Grishchuk; Klimnyuk; Zagrichuk; Kravchenyuk; Kolomiets; Gorbovoi
Pharmaceutical Chemistry Journal, 1999 , vol. 33, # 3 p. 143 - 144
反应条件
copper diacetate in water; acetone
T=5 - 10°C; Arylation;
参考文献
Grishchuk; Klimnyuk; Zagrichuk; Kravchenyuk; Kolomiets; Gorbovoi
Pharmaceutical Chemistry Journal, 1999 , vol. 33, # 3 p. 143 - 144
