8-甲氧基-2-氧代-2H-色烯-3-羧酸合成路线 (共 16 条)
反应条件
piperidinium acetate in ethanol 2 h; Heating;
参考文献
Garino, Cedrik; Tomita, Taisuke; Pietrancosta, Nicolas; Laras, Younes; Rosas, Roselyne; Herbette, Gaetan; Maigret, Bernard; Quelever, Gilles; Iwatsubo, Takeshi; Kraus, Jean-Louis
Journal of Medicinal Chemistry, 2006 , vol. 49, # 14 p. 4275 - 4285
反应条件
HZSM-5 zeolite Knoevenagel condensation; 0.05 h; microwave irradiation;
参考文献
Heravi, Majid M.; Hekmatshoar, Rahim; Emamgholizadeh, Maryam
Phosphorus, Sulfur and Silicon and the Related Elements, 2004 , vol. 179, # 9 p. 1893 - 1896
参考文献
Proceedings of the National Institute of Sciences of India, , vol. 6, p. 641,656
反应条件
1: ethanol; piperidine 2: aq. NaOH solution View Scheme
参考文献
Proceedings of the National Institute of Sciences of India, , vol. 6, p. 641,656
反应条件
1: 80 percent / diethyl ether / 1.) -70 grad C, 2 h, 2.) 0 grad C, 4 h, 3.) room temperature, 3 days 2: aq. NaOH View Scheme
参考文献
Tetrahedron Letters, , vol. 24, # 45 p. 5013 - 5016
参考文献
Tetrahedron Letters, , vol. 24, # 45 p. 5013 - 5016
反应条件
pyridine; sodium hydroxide
参考文献
Gazzetta Chimica Italiana, , vol. 84, p. 825,836
Annali di Chimica (Rome, Italy), , vol. 47, p. 557,573
反应条件
1: 12 h / Ambient temperature 2: 10ml H2O View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 1 p. 219 - 222
反应条件
1: 10ml TFA / 0.08 h / Ambient temperature 2: 12 h / Ambient temperature 3: 10ml H2O View Scheme
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 1 p. 219 - 222
参考文献
Journal of the Chemical Society, , vol. 105, p. 2384