N,O-双(三甲基硅烷基)三氟乙酰胺合成路线 (共 118 条)
反应条件
pyridine T=70°C; 1 h;
参考文献
Kotowska, Urszula; Isidorov, Valery A.
Central European Journal of Chemistry, 2011 , vol. 9, # 5 p. 813 - 824
反应条件
in acetonitrile 0.5 h; Ambient temperature;
参考文献
Journal of Medicinal Chemistry, , vol. 35, # 12 p. 2195 - 2201
反应条件
1: methyl vinyl ketone With HCo(CO)4 in dichloromethane T=-40°C; Reduction; 2: N,O-bis(trimethylsilyl) trifluoroacetamide in dichloromethane T=-30°C; silylation;
参考文献
Sisak, Attila
Journal of Organometallic Chemistry, 1999 , vol. 586, # 1 p. 48 - 53
反应条件
pyridine T=70°C; 1 h;
参考文献
Kotowska, Urszula; Isidorov, Valery A.
Central European Journal of Chemistry, 2011 , vol. 9, # 5 p. 813 - 824
反应条件
pyridine T=70°C; 1 h;
参考文献
Kotowska, Urszula; Isidorov, Valery A.
Central European Journal of Chemistry, 2011 , vol. 9, # 5 p. 813 - 824
反应条件
1: 4-methoxy-benzoic acid With cytochrome P450 enzyme CYP199A4 from Rhodopseudomonas palustris HaA2; nicotinamide adenine dinucleotide; bovine liver catalase in ethanol pH=7.4; Enzymatic reaction; 2: N,O-bis(trimethylsilyl) trifluoroacetamide With chloro-trimethyl-silane in acetonitrile 2 h;
参考文献
Bell, Stephen G.; Zhou, Ruimin; Yang, Wen; Tan, Adrian B. H.; Gentleman, Alexander S.; Wong, Luet-Lok; Zhou, Weihong
Chemistry - A European Journal, 2012 , vol. 18, # 52 p. 16677 - 16688
反应条件
in acetonitrile 2 h; Ambient temperature;
参考文献
Liu, Paul S.; Marquez, Victor E.; Driscoll, John S.; Fuller, Richard W.; McCormack, John J.
Journal of Medicinal Chemistry, 1981 , vol. 24, # 6 p. 662 - 666
反应条件
in acetonitrile 0.5 h; Ambient temperature;
参考文献
Kotowska, Urszula; Isidorov, Valery A.
Central European Journal of Chemistry, 2011 , vol. 9, # 5 p. 813 - 824
反应条件
pyridine T=80°C; 1 h;
参考文献
Rychlik, Michael
Journal of Mass Spectrometry, 2001 , vol. 36, # 5 p. 555 - 562
反应条件
1: 3,4-dimethoxy-benzoic acid With cytochrome P450 enzyme CYP199A4 from Rhodopseudomonas palustris HaA2; nicotinamide adenine dinucleotide; bovine liver catalase in ethanol pH=7.4; Enzymatic reaction; 2: N,O-bis(trimethylsilyl) trifluoroacetamide With chloro-trimethyl-silane in acetonitrile 2 h;
参考文献
Bell, Stephen G.; Zhou, Ruimin; Yang, Wen; Tan, Adrian B. H.; Gentleman, Alexander S.; Wong, Luet-Lok; Zhou, Weihong
Chemistry - A European Journal, 2012 , vol. 18, # 52 p. 16677 - 16688