N,O-双(三甲基硅烷基)三氟乙酰胺合成路线 (共 118 条)
反应条件
1: PFBHA; 1-hydroxy-2-propanone in water; acetonitrile T=20°C; Condensation; 24 h; 2: BSTFA in hexane; dichloromethane T=60°C; Substitution; 0.666667 h;
参考文献
Yu, Jianzhen; Flagan, Richard C.; Seinfeld, John H.
Environmental Science and Technology, 1998 , vol. 32, # 16 p. 2357 - 2370
反应条件
1: PFBHA; 2-oxo-propionic acid in water; acetonitrile T=20°C; Condensation; 24 h; 2: BSTFA in hexane; dichloromethane T=60°C; Substitution; 0.666667 h;
参考文献
Yu, Jianzhen; Flagan, Richard C.; Seinfeld, John H.
Environmental Science and Technology, 1998 , vol. 32, # 16 p. 2357 - 2370
反应条件
1: β-formylpropionic acid; PFBHA in water; acetonitrile T=20°C; Condensation; 24 h; 2: BSTFA in hexane; dichloromethane T=60°C; Substitution; 0.666667 h;
参考文献
Yu, Jianzhen; Flagan, Richard C.; Seinfeld, John H.
Environmental Science and Technology, 1998 , vol. 32, # 16 p. 2357 - 2370
反应条件
1: PFBHA; meta-hydroxybenzaldehyde in water; acetonitrile T=20°C; Condensation; 24 h; 2: BSTFA in hexane; dichloromethane T=60°C; Substitution; 0.666667 h;
参考文献
Yu, Jianzhen; Flagan, Richard C.; Seinfeld, John H.
Environmental Science and Technology, 1998 , vol. 32, # 16 p. 2357 - 2370
反应条件
1: PFBHA; alpha,beta dihydroxypropionaldehyde in water; acetonitrile T=20°C; Condensation; 24 h; 2: BSTFA in hexane; dichloromethane T=60°C; Substitution; 0.666667 h;
参考文献
Yu, Jianzhen; Flagan, Richard C.; Seinfeld, John H.
Environmental Science and Technology, 1998 , vol. 32, # 16 p. 2357 - 2370
反应条件
1: PFBHA; norpinalic acid in water; acetonitrile T=20°C; Condensation; 24 h; 2: BSTFA in hexane; dichloromethane T=60°C; Substitution; 0.666667 h;
参考文献
Yu, Jianzhen; Flagan, Richard C.; Seinfeld, John H.
Environmental Science and Technology, 1998 , vol. 32, # 16 p. 2357 - 2370
反应条件
1: norpinonic acid; PFBHA in water; acetonitrile T=20°C; Condensation; 24 h; 2: BSTFA in hexane; dichloromethane T=60°C; Substitution; 0.666667 h;
参考文献
Yu, Jianzhen; Flagan, Richard C.; Seinfeld, John H.
Environmental Science and Technology, 1998 , vol. 32, # 16 p. 2357 - 2370
反应条件
1: 1R,cis 2,2-dimethyl-3-(2-oxo-propyl)-cyclopropane-1-carboxylic acid; PFBHA in water; acetonitrile T=20°C; Condensation; 24 h; 2: BSTFA in hexane; dichloromethane T=60°C; Substitution; 0.666667 h;
参考文献
Yu, Jianzhen; Flagan, Richard C.; Seinfeld, John H.
Environmental Science and Technology, 1998 , vol. 32, # 16 p. 2357 - 2370
反应条件
1: PFBHA; 3-caralic acid in water; acetonitrile T=20°C; Condensation; 24 h; 2: BSTFA in hexane; dichloromethane T=60°C; Substitution; 0.666667 h;
参考文献
Yu, Jianzhen; Flagan, Richard C.; Seinfeld, John H.
Environmental Science and Technology, 1998 , vol. 32, # 16 p. 2357 - 2370
反应条件
1: PFBHA; pinalic-3-acid in water; acetonitrile T=20°C; Condensation; 24 h; 2: BSTFA in hexane; dichloromethane T=60°C; Substitution; 0.666667 h;
参考文献
Yu, Jianzhen; Flagan, Richard C.; Seinfeld, John H.
Environmental Science and Technology, 1998 , vol. 32, # 16 p. 2357 - 2370