N,O-双(三甲基硅烷基)三氟乙酰胺合成路线 （共 118 条）
反应条件
1: cis-caronic acid; PFBHA in water; acetonitrile T=20°C; Condensation; 24 h; 2: BSTFA in hexane; dichloromethane T=60°C; Substitution; 0.666667 h;
参考文献
Yu, Jianzhen; Flagan, Richard C.; Seinfeld, John H.
Environmental Science and Technology, 1998 , vol. 32, # 16 p. 2357 - 2370
反应条件
1: 2-oxopropanedioic acid; PFBHA in water; acetonitrile T=20°C; Condensation; 24 h; 2: BSTFA in hexane; dichloromethane T=60°C; Substitution; 0.666667 h;
参考文献
Yu, Jianzhen; Flagan, Richard C.; Seinfeld, John H.
Environmental Science and Technology, 1998 , vol. 32, # 16 p. 2357 - 2370
反应条件
1: ketosuccinic acid; PFBHA in water; acetonitrile T=20°C; Condensation; 24 h; 2: BSTFA in hexane; dichloromethane T=60°C; Substitution; 0.666667 h;
参考文献
Yu, Jianzhen; Flagan, Richard C.; Seinfeld, John H.
Environmental Science and Technology, 1998 , vol. 32, # 16 p. 2357 - 2370
反应条件
1: acetone-1,3-dicarboxylic acid; PFBHA in water; acetonitrile T=20°C; Condensation; 24 h; 2: BSTFA in hexane; dichloromethane T=60°C; Substitution; 0.666667 h;
参考文献
Yu, Jianzhen; Flagan, Richard C.; Seinfeld, John H.
Environmental Science and Technology, 1998 , vol. 32, # 16 p. 2357 - 2370
反应条件
1: [14C]-2-Ketoglutaric acid; PFBHA in water; acetonitrile T=20°C; Condensation; 24 h; 2: BSTFA in hexane; dichloromethane T=60°C; Substitution; 0.666667 h;
参考文献
Yu, Jianzhen; Flagan, Richard C.; Seinfeld, John H.
Environmental Science and Technology, 1998 , vol. 32, # 16 p. 2357 - 2370
反应条件
in ethyl acetate Ambient temperature;
参考文献
Sakagami; Iwamatsu; Atsumi; Hatanaka
Chemical and Pharmaceutical Bulletin, 1990 , vol. 38, # 8 p. 2271 - 2273
反应条件
in hexane; dichloromethane T=60°C; Substitution; 0.666667 h;
参考文献
Yu, Jianzhen; Flagan, Richard C.; Seinfeld, John H.
Environmental Science and Technology, 1998 , vol. 32, # 16 p. 2357 - 2370
反应条件
pyridine T=70°C; 1 h;
参考文献
Kotowska, Urszula; Isidorov, Valery A.
Central European Journal of Chemistry, 2011 , vol. 9, # 5 p. 813 - 824
反应条件
in acetonitrile T=78 - 80°C; 3 h;
参考文献
Bennek, John A.; Gray, Gary R.
Journal of Organic Chemistry, 1987 , vol. 52, # 5 p. 892 - 897
反应条件
1: 2-chloroethyl ethyl thioether With N-hexadecyl-N,N,N-trimethylammonium bromide in hexane; water; butan-1-ol T=25°C; 0.5 h; 2: N,O-bis(trimethylsilyl) trifluoroacetamide With sodium hydroxide in acetonitrile T=70°C; pH=10; 0.5 h; Mechanism;
参考文献
Mei-Ling, Lei; Hai-Ling, Xi; Ming, Shen; Ling, Yuan; Shi-Tong, Han
Phosphorus, Sulfur and Silicon and the Related Elements, 2014 , vol. 189, # 3 p. 387 - 393
