1-苯甲酰基氮杂丁烷-3-酮合成路线 （共 5 条）
反应条件
ozone in dichloromethane T=-40°C; 2 h;
参考文献
Marchand, Alan P.; Devasagayaraj, Arokiasamy
Synthetic Communications, 1999 , vol. 29, # 5 p. 885 - 890
反应条件
triethylamine in dimethyl sulfoxide
参考文献
Schering-Corporation
Patent: US4088644 A1, 1978 ;
反应条件
1: 74 percent / NaOH / diethyl ether / 12 h / 0 - 20 °C 2: 88 percent / activated Zn / tetrahydrofuran / 12 h / 65 °C 3: 68 percent / O3 / CH2Cl2 / 2 h / -40 °C View Scheme
参考文献
Marchand, Alan P.; Sharma; Rajagopal; Shukla, Rajesh; Mloston, Grzegorz; Bartnik, Romuald
Journal of Heterocyclic Chemistry, 1996 , vol. 33, # 3 p. 837 - 840
反应条件
1: 88 percent / activated Zn / tetrahydrofuran / 12 h / 65 °C 2: 68 percent / O3 / CH2Cl2 / 2 h / -40 °C View Scheme
参考文献
Marchand, Alan P.; Devasagayaraj, Arokiasamy
Synthetic Communications, 1999 , vol. 29, # 5 p. 885 - 890
反应条件
pyridine; 4-(N,N-dimethlyamino)pyridine in dichloromethane Ambient temperature; Yield given;
参考文献
Baumann, Hans; Duthaler, Rudolf O.
Helvetica Chimica Acta, 1988 , vol. 71, p. 1035 - 1041
