3,3',5,5'-四甲基联苯合成路线 (共 32 条)
反应条件
air; palladium diacetate in methanol T=20°C;
参考文献
Yamamoto, Yoshihiko; Suzuki, Ryo; Hattori, Kozo; Nishiyama, Hisao
Synlett, 2006 , # 7 p. 1027 - 1030
反应条件
N-[(1E,2E)-2-(2,6-dimethylphenyl)ethylidene]-2,6-dimethylphenylamine; niobium bromide; zinc in tetrahydrofuran T=70°C; 10 h; Inert atmosphere;
参考文献
Valaeva; Asachenko; Kulyabin; Flid; Voskoboinikov
Russian Journal of Organic Chemistry, 2011 , vol. 47, # 11 p. 1774 - 1776
反应条件
1,3-bis-(diphenylphosphino)propane; oxygen; palladium diacetate in dimethyl sulfoxide T=80°C; 24 h;
参考文献
Yoshida, Hiroto; Yamaryo, Yasuhito; Ohshita, Joji; Kunai, Atsutaka
Tetrahedron Letters, 2003 , vol. 44, # 8 p. 1541 - 1544
反应条件
sodium carbonate; 1,2-bis(2'-pyrazineethynyl)benzene palladium dichloride in water; acetonitrile T=70°C; Suzuki coupling; 6 h;
参考文献
Schultheiss, Nate; Barnes, Charles L.; Bosch, Eric
Synthetic Communications, 2004 , vol. 34, # 8 p. 1499 - 1505
反应条件
potassium carbonate; palladium dichloride in dimethyl sulfoxide T=20°C;
参考文献
Liu, Jin-Biao; Nie, Lin; Yan, Hui; Jiang, Li-Hua; Weng, Jiang; Lu, Gui
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 46 p. 8014 - 8017
反应条件
sodium carbonate; palladium dichloride; silver(l) oxide in methanol T=20°C; 0.666667 h; Ultrasound irradiation;
参考文献
Singh, Fateh V.; Stefani, Helio A.
Tetrahedron Letters, 2010 , vol. 51, # 5 p. 863 - 867
反应条件
palladium diacetate in tetrahydrofuran T=20 - 58°C; 2 h; Inert atmosphere;
参考文献
Chemical Communications, , vol. 47, # 18 p. 5172 - 5174
反应条件
palladium diacetate; 2-tBuP-3,4,5,6-Me4-2',4',6'-tri-isopropylbiphenyl; caesium carbonate in toluene T=90°C; 24 h;
参考文献
Journal of the American Chemical Society, , vol. 127, # 22 p. 8146 - 8149
反应条件
triethylamine in toluene T=0 - 20°C; 2 h; Inert atmosphere; Reagent/catalyst;
参考文献
Chemistry - A European Journal, , vol. 19, # 20 p. 6225 - 6229
参考文献
Journal of the American Chemical Society, , vol. 80, p. 2322,2324