3,3',5,5'-四甲基联苯合成路线 （共 32 条）
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium hydroxide in tert-butyl methyl ether; water T=80°C; Suzuki-Miyaura coupling; 3 h;
参考文献
Synlett, , # 1 p. 147 - 150
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium hydroxide in tert-butyl methyl ether; water T=80°C; Suzuki-Miyaura coupling; 3 h;
参考文献
Synlett, , # 1 p. 147 - 150
反应条件
(1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium hydroxide in tert-butyl methyl ether; water T=80°C; Suzuki-Miyaura coupling; 3 h;
参考文献
Synlett, , # 1 p. 147 - 150
反应条件
C34H38Cl2N4Pd; caesium carbonate in 1,4-dioxane T=100°C; Suzuki coupling; 25 h;
参考文献
Dalton Transactions, , # 11 p. 2020 - 2028
反应条件
1-(2-di-tert-butylphosphino-3,4,5,6-tetramethylphenyl)-2-neopentylnaphthalene; palladium diacetate; caesium carbonate; tributyl-amine T=90°C; 24 h; Product distribution; Further Variations:Reagents;
参考文献
Journal of the American Chemical Society, , vol. 127, # 22 p. 8146 - 8149
反应条件
1: ortho-cresol With tris-(dibenzylideneacetone)dipalladium(0); sodium hydroxide; di-tert-butyl(2′,4′,6′-triisopropylbiphenyl-2-yl)phosphine in 1,4-dioxane; polyethylene glycol; water T=80°C; 1 h; 2: 1-bromo-3,5-dimethyl-benzene in 1,4-dioxane; polyethylene glycol; water T=80°C;
参考文献
Journal of Physical Chemistry A, , vol. 114, # 11 p. 3932 - 3938
反应条件
1.1: cobalt(II) dibromide; trifluoroacetic acid; 3-chloroprop-1-ene / acetonitrile / 0.05 h / 20 °C 1.2: 20 °C 2.1: triethylamine / toluene / 2 h / 0 - 20 °C / |Inert atmosphere View Scheme
参考文献
Chemistry - A European Journal, , vol. 19, # 20 p. 6225 - 6229
参考文献
Tetrahedron Letters, , vol. 23, # 40 p. 4077 - 4078
反应条件
(i) nPrCO2H, (ii) Pt-C; Multistep reaction;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 22, p. 2351
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , vol. 22, p. 2399 - 2400
反应条件
2: (i) nPrCO2H, (ii) Pt-C View Scheme
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 22, p. 2351
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , vol. 22, p. 2399 - 2400
