2-(二叔丁基磷)-1,1'-联萘合成路线 (共 2 条)
反应条件
1: 2-bromo-[1,1']dinaphthyl With magnesium in tetrahydrofuran T=65°C; 1.3 h; 2: chlorodi-tert-butylphosphine With copper(l) chloride in tetrahydrofuran T=65°C; 26 h; Further stages.;
参考文献
Toracca, Karen E.; Kuwabe, Shin-Itsu; Buchwald, Stephen L.
Journal of the American Chemical Society, 2000 , vol. 122, # 51 p. 12907 - 12908
反应条件
copper(l) chloride in tetrahydrofuran T=65°C; 26 h;
参考文献
Kuwabe; Torraca; Buchwald
Journal of the American Chemical Society, 2001 , vol. 123, # 49 p. 12202 - 12206