1: With triethylsilane; trifluoroacetic acid in dichloromethane T=20°C; Reduction; 1.5 h; 2: With borane in tetrahydrofuran T=0 - 20°C; Addition; 3: With acetic acid T=20°C; Substitution; 6 h; Further stages.;
参考文献
Wolfe, John P.; Tomori, Hiroshi; Sadighi, Joseph P.; Yin, Jingjun; Buchwald, Stephen L.
Journal of Organic Chemistry, 2000 , vol. 65, # 4 p. 1158 - 1174
triethylsilane; trifluoroacetic acid in dichloromethane T=20°C; Dehydration; 1.5 h; Title compound not separated from byproducts.;
参考文献
Wolfe, John P.; Tomori, Hiroshi; Sadighi, Joseph P.; Yin, Jingjun; Buchwald, Stephen L.
Journal of Organic Chemistry, 2000 , vol. 65, # 4 p. 1158 - 1174