4-乙炔-2,6-二甲基-苯胺合成路线 (共 3 条)
反应条件
potassium hydroxide in toluene Elimination; 9 h; Heating;
参考文献
Jeong, Kyu-Sung; Cho, Young Lag; Chang, Sung-Youn; Park, Tae-Yoon; Song, Jung Uk
Journal of Organic Chemistry, 1999 , vol. 64, # 26 p. 9459 - 9466
反应条件
1: 100 percent / piperidine / Pd(PPh3)4; CuI / various solvent(s) / 16 h / 20 °C 2: 89 percent / aq. NaOH / tetrahydrofuran; methanol / 3 h View Scheme
参考文献
Azov, Vladimir A.; Schlegel, Anna; Diederich, Francois
Bulletin of the Chemical Society of Japan, 2006 , vol. 79, # 12 p. 1926 - 1940
反应条件
1: 66 percent / diethylamine; CuI; (PPh3)4Pd / 48 h / Heating 2: 91 percent / potassium hydroxide / toluene / 9 h / Heating View Scheme
参考文献
Jeong, Kyu-Sung; Cho, Young Lag; Chang, Sung-Youn; Park, Tae-Yoon; Song, Jung Uk
Journal of Organic Chemistry, 1999 , vol. 64, # 26 p. 9459 - 9466