ammonia
byproducts: {CH3NH3}SH, cyclo-1,2-dithia-4-aza-3,5-diboranes, cyclo-1-thia-3,5-diaza-2,4,6-triboranes; ratio of products depends on concentration; in cold;
参考文献
Gmelin Handbook: B: B Comp.SVol.1/3, 10.7.2.2, page 68 - 69
in diethyl ether
(Ar); Schlenk techniques; Me2NH condensed into Et2O soln. of Me2B2S3 at -78°C; warmed to room temp.; refluxed for 16 h; vac. evapn.; vac. distn.; detn. by NMR;
参考文献
Noeth, Heinrich; Taeger, Tilman
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, 2010 , vol. 65, # 2 p. 173 - 177
