5H-二苯并[a,d]环庚烯合成路线 （共 55 条）
反应条件
monohydrazine sulfate; hydrazine
Heating; Yield given;
参考文献
Wright; Platz
Journal of the American Chemical Society, 1984 , vol. 106, # 15 p. 4175 - 4180
参考文献
Rigaudy; Tardieu
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1955 , vol. 240, p. 1347
反应条件
naphthalene in neat (no solvent)
T=430°C; P=0.05 Torr; 1 h; Product distribution;
参考文献
Pomerantz, Martin; Combs, Gerald L.; Fink, Rina
Journal of Organic Chemistry, 1980 , vol. 45, # 1 p. 143 - 149
反应条件
quartz
T=550 - 800°C; Inert atmospherePyrolysis;
参考文献
Istrati, Daniela; Parvulescu, Luminitza; Popescu, Angela; Mihaiescu, Dan; Badea, Florin
Revue Roumaine de Chimie, 2010 , vol. 55, # 10 p. 711 - 714
反应条件
quartz
T=350 - 650°C; Inert atmospherePyrolysis;
参考文献
Istrati, Daniela; Parvulescu, Luminitza; Popescu, Angela; Mihaiescu, Dan; Badea, Florin
Revue Roumaine de Chimie, 2010 , vol. 55, # 10 p. 711 - 714
反应条件
aluminium trichloride; lithium tetrachloroaluminate
参考文献
Johnston, L. J.; Lobaugh, J.; Wintgens, V.
Journal of Physical Chemistry, 1989 , vol. 93, # 21 p. 7370 - 7374
反应条件
1: sodium tetrahydroborate; sodium hydroxide / methanol
2: quartz / 350 - 650 °C / Inert atmosphere; Pyrolysis
3: sodium tetrahydroborate; sodium hydroxide / methanol
4: H-ZSM-5 β mesoporous zeolite / 300 °C / Inert atmosphere; Pyrolysis
View Scheme
参考文献
Istrati, Daniela; Parvulescu, Luminitza; Popescu, Angela; Mihaiescu, Dan; Badea, Florin
Revue Roumaine de Chimie, 2010 , vol. 55, # 10 p. 711 - 714
反应条件
1: sodium tetrahydroborate; sodium hydroxide / methanol
2: quartz / 550 - 800 °C / Inert atmosphere; Pyrolysis
View Scheme
参考文献
Istrati, Daniela; Parvulescu, Luminitza; Popescu, Angela; Mihaiescu, Dan; Badea, Florin
Revue Roumaine de Chimie, 2010 , vol. 55, # 10 p. 711 - 714
反应条件
sodium azide in water
Ambient temperature; Rate constant;
参考文献
Johnston, L. J.; Lobaugh, J.; Wintgens, V.
Journal of Physical Chemistry, 1989 , vol. 93, # 21 p. 7370 - 7374
反应条件
in neat (no solvent)
T=345°C; P=0.05 Torr; 1 h; Product distribution;
参考文献
Pomerantz, Martin; Combs, Gerald L.; Fink, Rina
Journal of Organic Chemistry, 1980 , vol. 45, # 1 p. 143 - 149
