hydrogenchloride in hydrogenchloride

1: Na-Sn alloy 2: HCl / hydrogenchloride View Scheme

1: Na-Sn alloy 2: HCl / hydrogenchloride View Scheme

sodium in neat (no solvent) stoich. amt. of sodium (2 mol for 1 mol of ditin oxide), 120°C, 48 h; unreacted n-Pen6Sn2O was removed by filtration in pentane through a short SiO2 column, n-Pen4Sn was removed by distn.;

sodium in neat (no solvent) stoich. amt. of sodium (2 mol for 1 mol of ditin oxide), 120°C, 48 h; unreacted n-Pen6Sn2O was removed by filtration in pentane through a short SiO2 column, n-Pen4Sn was removed by distn.;