1: With hydrogen; palladium on activated charcoal in methanol
P=3750.3 Torr;
2: With (+)-di-p-toluoyl-D-tartaric acid in methanol
T=22 - 25°C; 5 h;
3: With sodium carbonate in methyl acetate
T=20 - 25°C; 0.5 h;
参考文献
Prashad, Mahavir; Hu, Bin; Har, Denis; Repic, Oljan; Blacklock, Thomas J.; Acemoglu, Murat
Advanced Synthesis and Catalysis, 2001 , vol. 343, # 5 p. 461 - 472
1: With perchloric acid; hydrogen; acetic acid; palladium on activated charcoal
T=25°C; P=2585.81 Torr; 6 h;
2: With sodium hydrogencarbonate in dichloromethane; water
T=-2°C; pH=6.8 - 8; Further stages.;
参考文献
Waykole, Liladhar M.; McKenna, Joseph J.; Bach, Andrew; Prashad, Mahavir; Repic, Oljan; Blacklock, Thomas J.
Synthetic Communications, 2007 , vol. 37, # 9 p. 1445 - 1454
1: With perchloric acid; hydrogen; acetic acid; palladium on activated charcoal
P=2172.08 - 2585.81 Torr; 15.5 h;
2: With sodium hydrogencarbonate in dichloromethane; water
T=23°C; pH=8.0; Further stages.;
参考文献
Waykole, Liladhar M.; McKenna, Joseph J.; Bach, Andrew; Prashad, Mahavir; Repic, Oljan; Blacklock, Thomas J.
Synthetic Communications, 2007 , vol. 37, # 9 p. 1445 - 1454
