2,2,6,6-四甲基哌啶氧化物合成路线 (共 284 条)
反应条件
p-benozquinone in water-d2; acetonitrile T=25°C; Gibbs reaction; pH=9.2; 5 h; Product distributionKinetics; Further Variations:ReagentspH-values;
参考文献
Pallagi, Istvan; Toro, Andras; Horvath, Gyula
Journal of Organic Chemistry, 1999 , vol. 64, # 18 p. 6530 - 6540
反应条件
pyridine; [Mn2(μ-O)3(1,4,7-trimethyl-1,4,7-triazacyclononane)2](PF6)2; periodic acid in acetonitrile 0.25 h; Inert atmosphere;
参考文献
Amos, Ruth I. J.; Gourlay, Brendon S.; Yates, Brian F.; Schiesser, Carl H.; Lewis, Trevor W.; Smith, Jason A.
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 1 p. 170 - 176
反应条件
1: 2-cyclopentyl-benzo[1,3,2]dioxaborole With ethanol in dichloromethane T=0 - 20°C; 0.25 h; Inert atmosphere; 2: N-phenyl-maleimide; 2,2,6,6-tetramethyl-1-piperidinyloxy, free radical With N,N'-dimethyl-N,N'-propyleneurea in dichloromethane T=20°C; Inert atmosphere;
参考文献
Birch, Peter; Parsons, Andrew F.; Cross, Paul
Tetrahedron Letters, 2012 , vol. 53, # 7 p. 822 - 824
反应条件
magnesium in diethyl ether T=34°C;
参考文献
Lawrence, Lynnette M.; Whitesides, George M.
Journal of the American Chemical Society, 1980 , vol. 102, # 7 p. 2493 - 2494
反应条件
Dess-Martin periodane in diethyl ether T=20°C; Inert atmosphere;
参考文献
Sorin, Geoffroy; Martinezmallorquin, Rocio; Contie, Yohan; Baralle, Alexandre; Malacria, Max; Goddard, Jean-Philippe; Fensterbank, Louis
Angewandte Chemie - International Edition, 2010 , vol. 49, # 46 p. 8721 - 8723
反应条件
magnesium in diethyl ether T=34°C; other reagens, reagens ratio; Product distribution;
参考文献
Lawrence, Lynnette M.; Whitesides, George M.
Journal of the American Chemical Society, 1980 , vol. 102, # 7 p. 2493 - 2494
反应条件
in 2,2,4-trimethylpentane T=19°C; other solvents and other temp.; Rate constant;
参考文献
Bowry; Ingold
Journal of the American Chemical Society, 1992 , vol. 114, # 13 p. 4992 - 4996
反应条件
in diethyl ether T=34°C; other reagens, reagens ratio, mode of addition; Product distribution;
参考文献
Lawrence, Lynnette M.; Whitesides, George M.
Journal of the American Chemical Society, 1980 , vol. 102, # 7 p. 2493 - 2494
反应条件
in decane T=150°C; Oxidation; 2.5 h; Product distributionKinetics;
参考文献
Mar'in, Alexander; Damiani, Elisabetta; Canestrari, Stefania; Dubs, Paul; Greci, Lucedio
Journal of the Chemical Society. Perkin Transactions 2, 1999 , # 7 p. 1363 - 1367
反应条件
water; periodic acid in acetonitrile T=0 - 20°C; nitrogen bubbling; Product distribution; Further Variations:Reagents;
参考文献
Amos, Ruth I. J.; Gourlay, Brendon S.; Schiesser, Carl H.; Smith, Jason A.; Yates, Brian F.
Chemical Communications, 2008 , # 14 p. 1695 - 1697